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Rh(III)-Catalyzed Dual C-H Functionalization/Cyclization Cascade by a Removable Directing Group: A Method for Synthesis of Polycyclic Fused Pyrano[de]Isochromenes

文献类型：期刊论文

作者Shu, Zhihao1,2,3; Zhou, Jianhui2,3; Li, Junyou2,3; Cheng, Yilang2,3; Liu, Hong1,2,3; Wang, Dechuan1; Zhou, Yu2,3
刊名JOURNAL OF ORGANIC CHEMISTRY
出版日期2020-10-02
卷号85期号:19页码:12097-12107
ISSN号0022-3263
DOI10.1021/acs.joc.0c01228
通讯作者Wang, Dechuan(wdc@cpu.edu.cn) ; Zhou, Yu(zhouyu@simm.ac.cn)
英文摘要An interesting Rh(III)-catalyzed dual C-H functionalization/cyclization cascade of azomethine imine with diazophosphonate by a removable directing group for the synthesis of highly fused pyrano[de]isochromene has been achieved. The transformation shows that the desired pyrano[de]isochromenes with two oxygen atoms on its core scaffold could be constructed with good to excellent yields (up to 86%) via a facile one-pot, multiple-step cascade reaction, along with broad generality and versatility.
WOS关键词RELAY CARBENOID FUNCTIONALIZATION ; DIAZO-COMPOUNDS ; BOND ACTIVATION ; MORUS-ALBA ; CYCLIZATION ; ACCESS ; ACTIVATION/CYCLIZATION ; BENZAMIDES ; SYNTHONS
资助项目National Natural Science Foundation of China[21672232] ; National Natural Science Foundation of China[21632008] ; National Natural Science Foundation of China[81620108027] ; Strategic Priority Research Program of the Chinese Academy of Sciences[XDA12040217]
WOS研究方向Chemistry
语种英语
WOS记录号WOS:000577156600009
出版者AMER CHEMICAL SOC
源URL[http://119.78.100.183/handle/2S10ELR8/291422]  
专题新药研究国家重点实验室
通讯作者Wang, Dechuan; Zhou, Yu
作者单位1.China Pharmaceut Univ, Sch Sci, Nanjing 211198, Peoples R China
2.Chinese Acad Sci, Shanghai Inst Mat Med, State Key Lab Drug Res, Shanghai 201203, Peoples R China
3.Chinese Acad Sci, Shanghai Inst Mat Med, Key Lab Receptor Res, Shanghai 201203, Peoples R China
推荐引用方式
GB/T 7714		 Shu, Zhihao,Zhou, Jianhui,Li, Junyou,et al. Rh(III)-Catalyzed Dual C-H Functionalization/Cyclization Cascade by a Removable Directing Group: A Method for Synthesis of Polycyclic Fused Pyrano[de]Isochromenes[J]. JOURNAL OF ORGANIC CHEMISTRY,2020,85(19):12097-12107.
APA Shu, Zhihao.,Zhou, Jianhui.,Li, Junyou.,Cheng, Yilang.,Liu, Hong.,...&Zhou, Yu.(2020).Rh(III)-Catalyzed Dual C-H Functionalization/Cyclization Cascade by a Removable Directing Group: A Method for Synthesis of Polycyclic Fused Pyrano[de]Isochromenes.JOURNAL OF ORGANIC CHEMISTRY,85(19),12097-12107.
MLA Shu, Zhihao,et al."Rh(III)-Catalyzed Dual C-H Functionalization/Cyclization Cascade by a Removable Directing Group: A Method for Synthesis of Polycyclic Fused Pyrano[de]Isochromenes".JOURNAL OF ORGANIC CHEMISTRY 85.19(2020):12097-12107.

入库方式： OAI收割

来源：上海药物研究所

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