Three-Dimensional Microstructure of epsilon-Fe2O3 Crystals in Ancient Chinese Sauce Glaze Porcelain Revealed by Focused Ion Beam Scanning Electron Microscopy
文献类型：期刊论文
| 作者 | Wang, LH; Wang, Y; Zhang, ML; Li, QJ; Wu, JM; Liu, Z; Li, L; Wei, XJ |
| 刊名 | ANALYTICAL CHEMISTRY
 |
| 出版日期 | 2019 |
| 卷号 | 91期号:20页码:13054-13061 |
| 关键词 | GIANT COERCIVE FIELD GROWTH-MECHANISM LUSTER POTTERY NANOPARTICLES FE3O4 OXIDE |
| ISSN号 | 0003-2700 |
| DOI | 10.1021/acs.analchem.9b03244 |
| 文献子类 | 期刊论文 |
| 英文摘要 | Ancient Chinese sauce glaze porcelain has recently received growing attention for the discovery of epsilon iron oxide (epsilon-Fe2O3) crystals in glaze. In this work, we first confirm the presence of epsilon-Fe2O3 microcrystals, in large quantiteis, in sauce glaze porcelain fired at the Qlizhen kiln in Jiangxi province during the Southern Song dynasty. We then employed focused ion beam scanning electron microscopy (FIB-SEM) to investigate the three-dimensional microstructure of epsilon-Fe2O3 microcrystals, which revealed three well-separated layers (labeled, respectively, as LY1, LY2, and LY3 from the glaze surface to inside) under the glaze surface. Specifically, LY1 consists of well-defined dendritic fractal structure with high ordered branches at micrometers scale, LY2 has spherical or irregular-shaped particles at nanometers scale, while LY3 consists of dendrites with four, six, or eight primary branches ranging from several nanometers to around 1 mu m. Given these findings, we proposed a process for the possible growth of epsilon-Fe2O3 microcrystals in ancient Chinese sauce glaze. |
| 语种 | 英语 |
| 源URL | [http://ir.sinap.ac.cn/handle/331007/32254]  |
| 专题 | 上海应用物理研究所_中科院上海应用物理研究所2011-2017年 |
| 作者单位 | 1.Chinese Acad Sci, Shanghai Synchrotron Radiat Facil, Zhangjiang Lab ZJLab, Shanghai Adv Res Inst, Shanghai 201210, Peoples R China; 2.Chinese Acad Sci, Shanghai Inst Appl Phys, Shanghai 201204, Peoples R China; 3.Jingdezhen Ceram Inst, Inst Ancient Ceram, Jingdezhen City, Jiangxi, Peoples R China |
| 推荐引用方式 GB/T 7714 | Wang, LH,Wang, Y,Zhang, ML,et al. Three-Dimensional Microstructure of epsilon-Fe2O3 Crystals in Ancient Chinese Sauce Glaze Porcelain Revealed by Focused Ion Beam Scanning Electron Microscopy[J]. ANALYTICAL CHEMISTRY,2019,91(20):13054-13061. |
| APA | Wang, LH.,Wang, Y.,Zhang, ML.,Li, QJ.,Wu, JM.,...&Wei, XJ.(2019).Three-Dimensional Microstructure of epsilon-Fe2O3 Crystals in Ancient Chinese Sauce Glaze Porcelain Revealed by Focused Ion Beam Scanning Electron Microscopy.ANALYTICAL CHEMISTRY,91(20),13054-13061. |
| MLA | Wang, LH,et al."Three-Dimensional Microstructure of epsilon-Fe2O3 Crystals in Ancient Chinese Sauce Glaze Porcelain Revealed by Focused Ion Beam Scanning Electron Microscopy".ANALYTICAL CHEMISTRY 91.20(2019):13054-13061. |
入库方式： OAI收割
来源：上海应用物理研究所
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