Synthesis of 3,6-bisubstituted phenyl-bi-1,2,4-triazolo[3,4-b]1,3,4-thiadiazole derivatives
文献类型：期刊论文
| 作者 | Qian Jian-Hua; Liu Lin; Wang Dao-Lin; Xing Jin-Juan |
| 刊名 | CHINESE JOURNAL OF ORGANIC CHEMISTRY
 |
| 出版日期 | 2006-12-01 |
| 卷号 | 26期号:12页码:1720-1722 |
| 关键词 | POCl3 2,5-bihydrazino-1,3,4-thiadiazol triazolo-1,3,4-thiadiazole mechanism |
| ISSN号 | 0253-2786 |
| 通讯作者 | Qian Jian-Hua(jhqian1964@sohu.com) |
| 英文摘要 | 2,5-Bihydrazino-1,3,4-thiadiazole was synthesized by substitution of 2,5-bimercapto-1,3,4-thiadiazole with hydrazine hydrate and reacted with benzoyl chloride to give 2,5-biacylhydrazino-1,3,4-thiadiazole, which was further ring-closed by POCl3 as cyclization agent to synthesize 3,6-bisubstituted phenyl-bi-1,2,4-triazolo[3,4-b]-1,3,4-thiadiazole derivatives. The novel compounds were confirmed by elemental analysis, IR, H-1 NMR and MS spectra. The mechanism of cycloreaction was also discussed. |
| WOS研究方向 | Chemistry |
| 语种 | 英语 |
| WOS记录号 | WOS:000242750700019 |
| 出版者 | SCIENCE CHINA PRESS |
| 源URL | [http://ir.imr.ac.cn/handle/321006/88132]  |
| 专题 | 金属研究所_中国科学院金属研究所 |
| 通讯作者 | Qian Jian-Hua |
| 作者单位 | 1.Chinese Acad Sci, Inst Met Res, State Key Lab Corros & Protect, Shenyang 110016, Peoples R China 2.Bohai Univ, Prov Key Lab Appl Chem, Jinzhou 121000, Peoples R China |
| 推荐引用方式 GB/T 7714 | Qian Jian-Hua,Liu Lin,Wang Dao-Lin,et al. Synthesis of 3,6-bisubstituted phenyl-bi-1,2,4-triazolo[3,4-b]1,3,4-thiadiazole derivatives[J]. CHINESE JOURNAL OF ORGANIC CHEMISTRY,2006,26(12):1720-1722. |
| APA | Qian Jian-Hua,Liu Lin,Wang Dao-Lin,&Xing Jin-Juan.(2006).Synthesis of 3,6-bisubstituted phenyl-bi-1,2,4-triazolo[3,4-b]1,3,4-thiadiazole derivatives.CHINESE JOURNAL OF ORGANIC CHEMISTRY,26(12),1720-1722. |
| MLA | Qian Jian-Hua,et al."Synthesis of 3,6-bisubstituted phenyl-bi-1,2,4-triazolo[3,4-b]1,3,4-thiadiazole derivatives".CHINESE JOURNAL OF ORGANIC CHEMISTRY 26.12(2006):1720-1722. |
入库方式： OAI收割
来源：金属研究所
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