Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying
文献类型:期刊论文
作者 | Yang Fen2; Zhang Xuejun4; Tian Fang2; Wu Xu2; Gan Fuxing2 |
刊名 | CHINESE JOURNAL OF AERONAUTICS
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出版日期 | 2007 |
卷号 | 20期号:2页码:181-186 |
关键词 | antimony-doped tin oxide ion-exchange iso-amyl acetate dispersivity |
ISSN号 | 1000-9361 |
其他题名 | Preparation of Highly Dispersed Antimony-doped Tin Oxide Nano-powder via Ion-exchange Hydrolysis of SnCl_4 and SbCl_3 and Azeotropic Drying |
英文摘要 | Antimony-doped tin hydroxide colloid precipitates have been synthesized by hydrolysis of SnCl4 and SbCl3 using: (1) an ion-exchange hydrolysis to remove chlorine ions, and (2) isoamyl acetate as an azeotropic solvent to obviate water. The obtained dried powder is of high dispersivity without any need for further grinding. The size and dispersivity of the final particles are investigated with the aid of TG-DTA, BET, XRD and TEM. After having calcined, the antimony-doped tin oxide nanopowder possesses a tetragonal rutile structure with high dispersivity, uniform particles and low hard agglomeration. |
语种 | 英语 |
CSCD记录号 | CSCD:2911963 |
源URL | [http://ir.imr.ac.cn/handle/321006/144194] ![]() |
专题 | 金属研究所_中国科学院金属研究所 |
作者单位 | 1.中国科学院金属研究所 2.武汉大学 3.曲靖师范学院 4.贵州大学 |
推荐引用方式 GB/T 7714 | Yang Fen,Zhang Xuejun,Tian Fang,et al. Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying[J]. CHINESE JOURNAL OF AERONAUTICS,2007,20(2):181-186. |
APA | Yang Fen,Zhang Xuejun,Tian Fang,Wu Xu,&Gan Fuxing.(2007).Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying.CHINESE JOURNAL OF AERONAUTICS,20(2),181-186. |
MLA | Yang Fen,et al."Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying".CHINESE JOURNAL OF AERONAUTICS 20.2(2007):181-186. |
入库方式: OAI收割
来源:金属研究所
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