PREPARATION AND CHARACTERIZATION OF CaB6 BY MOLTEN SALT ELECTROLYSIS
文献类型：期刊论文
| 作者 | Wang Xu; Zhai Yuchun; Xie Hongwei |
| 刊名 | ACTA METALLURGICA SINICA
 |
| 出版日期 | 2008 |
| 卷号 | 44期号:10页码:1243-1246 |
| 关键词 | ELECTROCHEMICAL REDUCTION TITANIUM-DIOXIDE CALCIUM-CHLORIDE EXTRACTION ALLOYS POWDER molten salt electrolysis molten salt system CaB6 diffusion rate cyclic voltammetry |
| ISSN号 | 0412-1961 |
| 其他题名 | PREPARATION AND CHARACTERIZATION OF CaB_6 BY MOLTEN SALT ELECTROLYSIS |
| 英文摘要 | CaB6 powder was synthesized by molten salt electrolysis method, and the effects of synthesis temperature, electrolysis voltage and time on the phase composition, particle size and shape of cathode products were analyzed by XRD and SEM. The experimental results show that the best synthesis conditions of CaB6 powder in CaCl2 Molten salt system are: environment of argon, voltage of 3.0 V, temperature of 900 degrees C for 30 h, under which the range of CaB6 crystal size is 2-8 mu m and the morphology of particles is cuboid massive shape. Using cyclic voltammetry in cathode process, it is proved that the electrolysis process is controlled by the diffusion rate of borate to the cathode. |
| 语种 | 英语 |
| CSCD记录号 | CSCD:3420311 |
| 源URL | [http://ir.imr.ac.cn/handle/321006/152814]  |
| 专题 | 金属研究所_中国科学院金属研究所 |
| 作者单位 | 中国科学院金属研究所 |
| 推荐引用方式 GB/T 7714 | Wang Xu,Zhai Yuchun,Xie Hongwei. PREPARATION AND CHARACTERIZATION OF CaB6 BY MOLTEN SALT ELECTROLYSIS[J]. ACTA METALLURGICA SINICA,2008,44(10):1243-1246. |
| APA | Wang Xu,Zhai Yuchun,&Xie Hongwei.(2008).PREPARATION AND CHARACTERIZATION OF CaB6 BY MOLTEN SALT ELECTROLYSIS.ACTA METALLURGICA SINICA,44(10),1243-1246. |
| MLA | Wang Xu,et al."PREPARATION AND CHARACTERIZATION OF CaB6 BY MOLTEN SALT ELECTROLYSIS".ACTA METALLURGICA SINICA 44.10(2008):1243-1246. |
入库方式： OAI收割
来源：金属研究所
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