Synthesis and Crystal Structure of Complex Pb（qina）2（DMSO）·H2O
文献类型：期刊论文
| 作者 | ZHANG WanZhong1; WEI DeZhou1; GAO EnJun2; SUN YaGuang2 |
| 刊名 | 结构化学
 |
| 出版日期 | 2007 |
| 卷号 | 26.0期号:003页码:357-360 |
| 关键词 | 铅配合物 喹拿啶酸 DMSO 合成 晶体结构 |
| ISSN号 | 0254-5861 |
| 其他题名 | Synthesis and Crystal Structure of Complex Pb（qina）2（DMSO）·H2O |
| 英文摘要 | A novel complex Pb（qina）2（DMSO）·H2O was synthesized, of which qinais the quinaldic acid radical and DMSO the dimethyl sulfoxide. Elemental analysis, IR spectra, and X-ray single-crystal diffraction were carried out to determine the composition and crystal structure. This complex belongs to monoclinic system, space group P121/n1, with a = 7.1553（17）, b = 17.543（2）, c = 17.306（2） A, β = 91.671（4）°, C22H20N206PbS, Mr = 647.65, Z = 4, V= 2171.5（6） A3, Dc= 1.981 g/cm^3, μ= 7.908 mm^-1, F（000） = 1248, -9≤h≤6, -23≤k≤19, -22≤1≤22, R= 0.0221 and wR= 0.0488. Weak coordinate bond is formed between oxygen atom in DMSO and Pb（ Ⅱ ）. There are also weak interactions, such as π-π interaction, hydrogen bonds and so on, among the complex molecules. |
| 语种 | 中文 |
| CSCD记录号 | CSCD:2729858 |
| 源URL | [http://ir.imr.ac.cn/handle/321006/157813]  |
| 专题 | 金属研究所_中国科学院金属研究所 |
| 作者单位 | 1.东北大学 2.中国科学院金属研究所 |
| 推荐引用方式 GB/T 7714 | ZHANG WanZhong,WEI DeZhou,GAO EnJun,等. Synthesis and Crystal Structure of Complex Pb（qina）2（DMSO）·H2O[J]. 结构化学,2007,26.0(003):357-360. |
| APA | ZHANG WanZhong,WEI DeZhou,GAO EnJun,&SUN YaGuang.(2007).Synthesis and Crystal Structure of Complex Pb（qina）2（DMSO）·H2O.结构化学,26.0(003),357-360. |
| MLA | ZHANG WanZhong,et al."Synthesis and Crystal Structure of Complex Pb（qina）2（DMSO）·H2O".结构化学 26.0.003(2007):357-360. |
入库方式： OAI收割
来源：金属研究所
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