Low-Temperature Molten Salt Synthesis and Characterization of Nanowire-Like TaB2 Powder
文献类型:期刊论文
作者 | Shah, Liaqat Ali |
刊名 | JOM
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出版日期 | 2021-01-04 |
页码 | 7 |
ISSN号 | 1047-4838 |
DOI | 10.1007/s11837-020-04509-6 |
英文摘要 | TaB2 nanopowder has been prepared by the molten salt synthesis (MSS) technique. Nanowire-like TaB2 nanopowder was successfully synthesized by reacting in the Ta2O5-MgB2 system using KCl/NaCl as reaction media. The impact of the firing temperature (800 degrees C to 1000 degrees C), firing time (1 h to 4 h), and ratio of reactants to salt (1:0, 1:2, 1:5, and 1:10) on the preparation of the TaB2 nanopowder was examined. The resultant powder samples were characterized by scanning electron microscopy (SEM), x-ray diffraction (XRD) analysis, transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), and surface area analysis (SAA). The results showed that the reaction involved in the formation of crystalline TaB2 nanopowder could be completed successfully at 1000 degrees C after 4 h of firing when the mass ratio of reactants to salt was 1:5. The resulting TaB2 nanopowders exhibited nanowire-like morphology. |
WOS关键词 | ZRB2 POWDERS ; COMPOSITES ; CERAMICS |
资助项目 | Chinese Academy of Sciences under the President's International Support Initiative (PIFI)[2017PE0006] |
WOS研究方向 | Materials Science ; Metallurgy & Metallurgical Engineering ; Mineralogy ; Mining & Mineral Processing |
语种 | 英语 |
WOS记录号 | WOS:000604800800001 |
出版者 | SPRINGER |
资助机构 | Chinese Academy of Sciences under the President's International Support Initiative (PIFI) |
源URL | [http://ir.ipe.ac.cn/handle/122111/43082] ![]() |
专题 | 中国科学院过程工程研究所 |
通讯作者 | Shah, Liaqat Ali |
作者单位 | Chinese Acad Sci, Inst Proc Engn, State Key Lab Multiphase Complex Syst, Beijing, Peoples R China |
推荐引用方式 GB/T 7714 | Shah, Liaqat Ali. Low-Temperature Molten Salt Synthesis and Characterization of Nanowire-Like TaB2 Powder[J]. JOM,2021:7. |
APA | Shah, Liaqat Ali.(2021).Low-Temperature Molten Salt Synthesis and Characterization of Nanowire-Like TaB2 Powder.JOM,7. |
MLA | Shah, Liaqat Ali."Low-Temperature Molten Salt Synthesis and Characterization of Nanowire-Like TaB2 Powder".JOM (2021):7. |
入库方式: OAI收割
来源:过程工程研究所
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