Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process
文献类型：期刊论文
| 作者 | Zhu Donghai; Nai Xueying ; Lan Shengjie; Dang Li; Liu Xin; Li Wu
|
| 刊名 | JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION
 |
| 出版日期 | 2017-10 |
| 卷号 | 32期号:5页码:1067-1071 |
| ISSN号 | 1000-2413 |
| DOI | 10.1007/s11595-017-1712-9 |
| 英文摘要 | Single crystalline calcium chloroborate (Ca2B5O9Cl) whiskers with uniform diameter have been fabricated by a two-step process. The precursor was firstly prepared by the sedimentation reaction between CaCl2, H3BO3 and NaOH aqueous solutions, and then sintered at different temperatures for 6 h with KCl as flux. The XRD indicates that the product synthesized at 600 degrees C is Orthorhombic Ca2B5O9Cl. SEM and TEM results show that the Ca2B5O9Cl is whisker with the diameter about 0.2-0.5 mu m and the length up to 15 mu m. SAED analysis shows that the whisker is single crystalline and grows along [001] direction. The possible formation process and growth mechanism were proposed. |
| 源URL | [http://ir.isl.ac.cn/handle/363002/34539]  |
| 专题 | 青海盐湖研究所_盐湖资源与化学实验室 |
| 推荐引用方式 GB/T 7714 | Zhu Donghai,Nai Xueying,Lan Shengjie,et al. Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process[J]. JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,2017,32(5):1067-1071. |
| APA | Zhu Donghai,Nai Xueying,Lan Shengjie,Dang Li,Liu Xin,&Li Wu.(2017).Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process.JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,32(5),1067-1071. |
| MLA | Zhu Donghai,et al."Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process".JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION 32.5(2017):1067-1071. |
入库方式： OAI收割
来源：青海盐湖研究所
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