Nafion assisted preparation of prussian blue nanoparticles and its application in electrochemical analysis of L-ascorbic acid
文献类型：期刊论文
| 作者 | Li, Yuqiong5; Pan, Fei3,4; Yin, Shengyan2; Tong, Chunyi1; Zhu, Rilong5; Li, Guoxi5 |
| 刊名 | MICROCHEMICAL JOURNAL
 |
| 出版日期 | 2022-06-01 |
| 卷号 | 177页码:7 |
| 关键词 | Prussian blue nanoparticles Nafion Single-precursor Sensor L-Ascorbic acid |
| ISSN号 | 0026-265X |
| DOI | 10.1016/j.microc.2022.107278 |
| 通讯作者 | Zhu, Rilong(zrlden@hnu.edu.cn) ; Li, Guoxi(liguoxi@hnu.edu.cn) |
| 英文摘要 | Due to the high sensitivity, simplicity and low cost, electrochemistry methods based on nanoparticles have been considered as an attractive technique for L-ascorbic acid. Herein, prussian blue nanoparticles (PBNPs) were synthesized by a fast and convenient synthesis strategy with Nafion and K4[Fe (CN)(6)] 3H2O. The PBNPs have uniform grain size of about 11.9 nm. PBNPs modified glassy carbon electrode (GCE) was used to construct electrochemical sensor for L-ascorbic acid (AA) detection and the optimization condition was studied. The electrochemical results indicate that PBNPs/GCE sensor shows a linear response to L-ascorbic acid in the range of 1-1100 mu M with a detection limit of 0.47 mu M and sensitivity of 22.9 mu A.mM(-1).cm(-2) at a working potential of 0.24 V (vs. SCE). The stability and reproducibility of the same PBNPs/GCE are RSD = 0.7% and RSD = 1.3%, respectively. The excellent characteristics of this sensor demonstrates it is a useful tool for accurate determination of L-ascorbic acid in medicine samples such as a vitamin C tablet and for Vitamin C chewable tablets. |
| WOS关键词 | NANOCOMPOSITE ; ELECTRODE ; SENSOR ; NANOCRYSTALS ; FABRICATION ; NANOCUBES ; BEHAVIOR ; SIZE |
| WOS研究方向 | Chemistry |
| 语种 | 英语 |
| WOS记录号 | WOS:000793749900005 |
| 资助机构 | Natural Science Foun-dation of Hunan Province ; Hunan Province Key RD Plan Project |
| 源URL | [http://ir.yic.ac.cn/handle/133337/31080]  |
| 专题 | 烟台海岸带研究所_中科院烟台海岸带研究所知识产出 |
| 通讯作者 | Zhu, Rilong; Li, Guoxi |
| 作者单位 | 1.Hunan Univ, Coll Biol, Changsha 410082, Hunan, Peoples R China 2.Hunan Normal Univ, Coll Life Sci, Changsha 410081, Peoples R China 3.Univ Chinese Acad Sci, Beijing 100049, Peoples R China 4.Chinese Acad Sci, Res Ctr Coastal Environm Engn Technol Shandong Pr, Yantai Inst Coastal Zone Res,Shandong Key Lab Coa, CAS Key Lab Coastal Environm Proc & Ecol Remediat, Yantai 264003, Peoples R China 5.Hunan Univ, Coll Chem & Chem Engn, Adv Catalyt Engn Res Ctr, Minist Educ, Changsha 410082, Hunan, Peoples R China |
| 推荐引用方式 GB/T 7714 | Li, Yuqiong,Pan, Fei,Yin, Shengyan,et al. Nafion assisted preparation of prussian blue nanoparticles and its application in electrochemical analysis of L-ascorbic acid[J]. MICROCHEMICAL JOURNAL,2022,177:7. |
| APA | Li, Yuqiong,Pan, Fei,Yin, Shengyan,Tong, Chunyi,Zhu, Rilong,&Li, Guoxi.(2022).Nafion assisted preparation of prussian blue nanoparticles and its application in electrochemical analysis of L-ascorbic acid.MICROCHEMICAL JOURNAL,177,7. |
| MLA | Li, Yuqiong,et al."Nafion assisted preparation of prussian blue nanoparticles and its application in electrochemical analysis of L-ascorbic acid".MICROCHEMICAL JOURNAL 177(2022):7. |
入库方式： OAI收割
来源：烟台海岸带研究所
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