Preparation of nanoscale WC powders by sol-gel synthesis and carbon monoxide carbonization
文献类型：期刊论文
| 作者 | Ke, J. G.1,2; Liu, R.1 ; Xie, Z. M.1; Sun, M.1; Jing, K.1,2; Zhang, G. F.1; Cheng, X.1,2; Liu, X. Q.1; Wang, X. P.1; Wu, X. B.1
|
| 刊名 | MATERIALS LETTERS
 |
| 出版日期 | 2022-07-01 |
| 卷号 | 318 |
| ISSN号 | 0167-577X |
| 关键词 | Tungsten carbide Sol-gel preparation Microstructure Nanopowder |
| DOI | 10.1016/j.matlet.2022.132143 |
| 通讯作者 | Liu, R.(liurui@issp.ac.cn) ; Fang, Q. F.(qffang@issp.ac.cn) |
| 英文摘要 | In this study, tungsten carbide (WC) nanopowders with an average size of about 10 nm were synthesized by a three-step process: the sol-gel preparation of nanoscale WO3, reduction and carbonization in carbon monoxide (CO) atmosphere and short time high-energy ball milling. The average particle size of the sol-gel synthesized WO3 precursor is about 31 nm. Through low-temperature reduction and carbonization at 700 degrees C in CO, spherical and dendritic WC powders were obtained. After high-energy ball milling at 800 rpm for 10 min and 20 min, the average particle size of WC decreases to 16 nm and 10 nm, respectively. This method provides a facile method for the preparation of nanoscale WC powders with the advantages of low cost, simple process and suitability for industrial production. |
| WOS关键词 | TUNGSTEN CARBIDE POWDER ; COMBUSTION SYNTHESIS ; REDUCTION |
| 资助项目 | National Key Research and Development Program of China[2019YFE03120001] ; National Key Research and Development Program of China[2017YFA0402800] ; National Natural Science Foundation of China[51971213] ; National Natural Science Foundation of China[52173303] ; HFIPS Director's Fund, Chinese Academy of Sciences[YZJJ202102] ; HFIPS Director's Fund, Chinese Academy of Sciences[YZJJZX202012] |
| WOS研究方向 | Materials Science ; Physics |
| 语种 | 英语 |
| 出版者 | ELSEVIER |
| WOS记录号 | WOS:000793245600001 |
| 资助机构 | National Key Research and Development Program of China ; National Natural Science Foundation of China ; HFIPS Director's Fund, Chinese Academy of Sciences |
| 源URL | [http://ir.hfcas.ac.cn:8080/handle/334002/130903]  |
| 专题 | 中国科学院合肥物质科学研究院 |
| 通讯作者 | Liu, R.; Fang, Q. F. |
| 作者单位 | 1.Chinese Acad Sci, Inst Solid State Phys, Key Lab Mat Phys, HFIPS, Hefei 230031, Peoples R China 2.Univ Sci & Technol China, Hefei 230026, Peoples R China |
| 推荐引用方式 GB/T 7714 | Ke, J. G.,Liu, R.,Xie, Z. M.,et al. Preparation of nanoscale WC powders by sol-gel synthesis and carbon monoxide carbonization[J]. MATERIALS LETTERS,2022,318. |
| APA | Ke, J. G..,Liu, R..,Xie, Z. M..,Sun, M..,Jing, K..,...&Fang, Q. F..(2022).Preparation of nanoscale WC powders by sol-gel synthesis and carbon monoxide carbonization.MATERIALS LETTERS,318. |
| MLA | Ke, J. G.,et al."Preparation of nanoscale WC powders by sol-gel synthesis and carbon monoxide carbonization".MATERIALS LETTERS 318(2022). |
入库方式： OAI收割
来源：合肥物质科学研究院
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。