Crystalline evolution of various CeO2 morphology via a solvothermal method
文献类型:会议论文
作者 | Fu, Cong2; Li, Ruixing2; Tang, Qing1; Li, Chengqiang2; Yin, Shu3; Sato, Tsugio3 |
出版日期 | 2011-04-01 |
关键词 | X ray diffraction - Cerium oxide |
卷号 | 37 |
期号 | 2023-02-05 |
DOI | 10.1007/s11164-011-0254-6 |
页码 | 319-327 |
英文摘要 | Preparation of cerium compounds with different structures and morphology is still a challenge in powder synthesis. CeOHCO3 and CeO2 have received widespread attention because of their potential applications. In this study, a solvothermal method with one-step precipitation was used to synthesize CeO2 with different structures and morphology without use of surfactant. The effects of different experimental conditions on the morphology of CeO2 were investigated. Both X-ray diffraction and SAED patterns revealed that products changed from a single CeOHCO3 phase to a mixture of CeOHCO3 and CeO2. A single CeO2 phase could always be obtained from CeOHCO3 by calcination in air at 673 K for 1 h. Moreover, the morphology of CeOHCO3 was retained. Thus CeO2 particles with different morphology, for example rod-like, prism-like, polygon-like, sphere-like, and cube-like, could be synthesized. Possible mechanisms of phase and morphology evolution are discussed. 漏 2011 Springer Science+Business Media B.V. |
项目编号 | Acknowledgments The authors appreciate financial support from the National Science Foundation of China (NSFC50752002) ; the Scientific Research Starting Foundation for Returned Overseas Chinese Scholars, Ministry of Education ; the Start-Up Fund for High-End Returned Overseas Talents, Ministry of Human Resources and Social Security, China and the Lab-Installation Foundation of Beihang University for New Teachers. |
资助机构 | Kluwer Academic Publishers |
学科主题 | Morphology |
源URL | [http://ir.ipe.ac.cn/handle/122111/59533] ![]() |
作者单位 | 1.Institute of Process Engineering, Chinese Academy of Sciences, Beijing 100190, China 2.Key Laboratory of Aerospace Materials and Performance (Ministry of Education), School of Materials Science and Engineering, Beihang University, Beijing 100191, China 3.Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1 Katahira, Aoba-ku, Sendai 980-8577, Japan |
推荐引用方式 GB/T 7714 | Fu, Cong,Li, Ruixing,Tang, Qing,et al. Crystalline evolution of various CeO2 morphology via a solvothermal method[C]. 见:. |
入库方式: OAI收割
来源:过程工程研究所
浏览0
下载0
收藏0
其他版本
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。