Effect of raw material size on the synthesis of silicon carbide
文献类型：期刊论文
| 作者 | Lu, Pengfei1,2; Jin, Zhihao1; Cui, Yanbin2; Xu, Guangwen1,2; Wu, Rongcheng2 |
| 刊名 | Huagong Xuebao/CIESC Journal
 |
| 出版日期 | 2021-04-01 |
| 卷号 | 72期号:4页码:2300-2308 |
| ISSN号 | 4381157 |
| 关键词 | Particle size - Coke - Morphology - Silicon oxides - Silicon carbide - Light transmission - Reaction intermediates - Tires - Carbothermal reduction - Crystal whiskers - Size distribution |
| DOI | 10.11949/0438-1157.20200981 |
| 英文摘要 | Using tire semi-coke as carbon source and silicon sand as silicon source, silicon carbide(SiC) was prepared by carbothermal reduction method at 1520. XRD, SEM and FTIR spectrometer were used to characterize the SiC prepared under different raw material particle size conditions. The influence law of raw material particle size on the phase, morphology, particle size and reaction degree of the synthesized SiC was investigated. The results show that the size of the raw material has a very important influence on the degree of synthesis reaction and the phase composition, morphology and size of the product.Within a certain particle size range, with the decrease of silicon sand particle size, SiC crystal type becomes complete and SiC whisker decreases gradually, while the SiC particle size distribution does not change significantly.With the increase of semi-coke size of tire, the product phase gradually becomes single, and the proportion of SiC particle size and whisker decreases gradually. In addition, by measuring the C/Si ratio in the product and confirming the presence of the intermediate product SiO, it is inferred that the formation mechanism of SiC particles is gas-solid (VS) reaction, while the formation mechanism of SiC whiskers is gas-gas(VV) reaction. 漏 2021, Editorial Board of CIESC Journal. All right reserved. |
| 学科主题 | Particle Size Analysis |
| 出版者 | Materials China |
| 源URL | [http://ir.ipe.ac.cn/handle/122111/60267]  |
| 作者单位 | 1.School of Mechanical and Power Engineering, Shenyang University of Chemical Technology, Shenyang; 110142, China 2.State Key Laboratory of Multiphase Complex Systems, Institute of Process Engineering, Chinese Academy of Sciences, Beijing; 100190, China |
| 推荐引用方式 GB/T 7714 | Lu, Pengfei,Jin, Zhihao,Cui, Yanbin,et al. Effect of raw material size on the synthesis of silicon carbide[J]. Huagong Xuebao/CIESC Journal,2021,72(4):2300-2308. |
| APA | Lu, Pengfei,Jin, Zhihao,Cui, Yanbin,Xu, Guangwen,&Wu, Rongcheng.(2021).Effect of raw material size on the synthesis of silicon carbide.Huagong Xuebao/CIESC Journal,72(4),2300-2308. |
| MLA | Lu, Pengfei,et al."Effect of raw material size on the synthesis of silicon carbide".Huagong Xuebao/CIESC Journal 72.4(2021):2300-2308. |
入库方式： OAI收割
来源：过程工程研究所
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