Higher ablative resistance performance of CF-ZrO2/ZrC composites by an in-situ sol-gel method
文献类型:期刊论文
作者 | Tong, Yuchen1,2; Hu, Zhufeng1,3; Wang, Min4; Yang, Chao1,2; Xu, Junbo1 |
刊名 | Composites Science and Technology |
出版日期 | 2022-08-18 |
卷号 | 227 |
ISSN号 | 2663538 |
关键词 | Ablation - Coatings - Heat transfer - Sol-gel process - Sol-gels - Thermolysis - Thermooxidation - Thickness measurement - Zirconia |
DOI | 10.1016/j.compscitech.2022.109625 |
英文摘要 | In the present study, CF-ZrO2/ZrC composites with controllable coating thickness were prepared by an in-situ sol-gel method. Through pretreatment, the carbon fibers surface changed from hydrophobic to hydrophilic and the polar groups on the surface significantly increased, which increased the interface affinity and ensured the stabilities of uniform ZrO2/ZrC coatings preparation. The coating layer increases the thickness of the composites, prolonged the mass and heat transfer on the composites surface. The dense ZrO2/ZrC coating prevents further oxidation of internal C by oxidative gas. As a result, after 4 cycles sol-gel, the mass ablation rate of the composite is decreased from 0.046 to 0.022 mg s鈭?, under the butane flame for 120s. And the thermal decomposition temperatures are 10.8%鈥?5% higher than those of the original carbon fiber. Thus, this in-situ sol-gel method is a feasible for preparing carbon fiber self-reinforced composites with uniform coating and designable structure, which can effectively improve the ablative resistance ability and thermal decomposition temperature of composites. 漏 2022 Elsevier Ltd |
学科主题 | Carbon Fibers |
项目编号 | We appreciate the financial support from the National Key Research and Development Program ( 2021YFB1716301 ), the National Natural Science Foundation of China ( 22035007 , 91934301 and 21878298 ), DNL Cooperation Fund, CAS ( DNL201902 ) and External Cooperation Program of BIC, Chinese Academy of Sciences ( 122111KYSB20190032 ). |
出版者 | Elsevier Ltd |
源URL | [http://ir.ipe.ac.cn/handle/122111/61240] |
作者单位 | 1.CAS Key Laboratory of Green Process and Engineering, Institute of Process Engineering, Chinese Academy of Sciences, Beijing; 100190, China 2.School of Chemical Engineering, University of Chinese Academy of Sciences, Beijing; 100049, China 3.School of Chemical Engineering, Sichuan University, Chengdu; 610065, China 4.Dynamic Machinery Institute of Inner Mongolia, Hohhot; 010010, China |
推荐引用方式 GB/T 7714 | Tong, Yuchen,Hu, Zhufeng,Wang, Min,et al. Higher ablative resistance performance of CF-ZrO2/ZrC composites by an in-situ sol-gel method[J]. Composites Science and Technology,2022,227. |
APA | Tong, Yuchen,Hu, Zhufeng,Wang, Min,Yang, Chao,&Xu, Junbo.(2022).Higher ablative resistance performance of CF-ZrO2/ZrC composites by an in-situ sol-gel method.Composites Science and Technology,227. |
MLA | Tong, Yuchen,et al."Higher ablative resistance performance of CF-ZrO2/ZrC composites by an in-situ sol-gel method".Composites Science and Technology 227(2022). |
入库方式: OAI收割
来源:过程工程研究所
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