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Convenient synthesis of N-alkyl-3,1-benzoxazin-2-ones from carbamate protected anthranil aldehydes and ketones via one-step alkylation/alkoxy rearrangement

文献类型：期刊论文

作者Tian, Guang1,2; Jin, Wei-Li2,3; Qin, Chuanguang1; Wang, Jie2,3,4
刊名ORGANIC & BIOMOLECULAR CHEMISTRY
出版日期2023-07-19
卷号21期号:28页码:5757-5761
ISSN号1477-0520
DOI10.1039/d3ob00812f
通讯作者Qin, Chuanguang(qinchg@nwpu.edu.cn) ; Wang, Jie(jiewang@simm.ac.cn)
英文摘要A practical and step-economical protocol was developed to prepare N-alkyl-3,1-benzoxazin-2-one derivatives from anthranil aldehydes and ketones via one-step alkylation/alkoxy rearrangement, where three new chemical bonds and one ring were constructed in a single step. Control studies revealed a stepwise mechanism and that the alkoxy rearrangement was an intermolecular process.
WOS关键词EFAVIRENZ ; ANALOGS
资助项目National Natural Science Foundation of China[22101290] ; Chinese Academy of Sciences ; Shanghai Institute of Materia Medica
WOS研究方向Chemistry
语种英语
WOS记录号WOS:001022039800001
出版者ROYAL SOC CHEMISTRY
源URL[http://119.78.100.183/handle/2S10ELR8/306397]  
专题中国科学院上海药物研究所
通讯作者Qin, Chuanguang; Wang, Jie
作者单位1.Northwestern Polytech Univ, Sch Chem & Chem Engn, Dept Chem, Shanxi Key Lab Polymer Sci & Technol,MOE Key Lab, Xian 710129, Peoples R China
2.Chinese Acad Sci, Shanghai Inst Mat Med, State Key Lab Chem Biol, Shanghai 201203, Peoples R China
3.Nanjing Univ Chinese Med, Sch Chinese Mat Med, Nanjing 210023, Peoples R China
4.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
推荐引用方式
GB/T 7714		 Tian, Guang,Jin, Wei-Li,Qin, Chuanguang,et al. Convenient synthesis of N-alkyl-3,1-benzoxazin-2-ones from carbamate protected anthranil aldehydes and ketones via one-step alkylation/alkoxy rearrangement[J]. ORGANIC & BIOMOLECULAR CHEMISTRY,2023,21(28):5757-5761.
APA Tian, Guang,Jin, Wei-Li,Qin, Chuanguang,&Wang, Jie.(2023).Convenient synthesis of N-alkyl-3,1-benzoxazin-2-ones from carbamate protected anthranil aldehydes and ketones via one-step alkylation/alkoxy rearrangement.ORGANIC & BIOMOLECULAR CHEMISTRY,21(28),5757-5761.
MLA Tian, Guang,et al."Convenient synthesis of N-alkyl-3,1-benzoxazin-2-ones from carbamate protected anthranil aldehydes and ketones via one-step alkylation/alkoxy rearrangement".ORGANIC & BIOMOLECULAR CHEMISTRY 21.28(2023):5757-5761.

入库方式： OAI收割

来源：上海药物研究所

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