TiCl4-catalyzed deoxygenative reduction of amides to amines using ammonia borane
文献类型：期刊论文
| 作者 | Zang, Yongjun1,3; Sui, Qibang2; Xu, Qilin1; Ma, Menghua1; Li, Guosi1; Zhu, Fucheng1 |
| 刊名 | TETRAHEDRON LETTERS
 |
| 出版日期 | 2023-07-11 |
| 卷号 | 124页码:4 |
| 关键词 | Deoxygenative reduction Amides Amines Ammonia borane |
| ISSN号 | 0040-4039 |
| DOI | 10.1016/j.tetlet.2023.154598 |
| 通讯作者 | Zang, Yongjun(zangyongjun@yeah.net) |
| 英文摘要 | A convenient and effective TiCl4-catalyzed procedure for the direct deoxygenative reduction of amides to corresponding amines has been developed using safe and stable ammonia borane (AB) as the reductant. This reduction protocol allows for a wide range of structurally diverse amine products in moderate to excellent yields, various functional groups such as halogen, nitro, and hydroxy groups were well toler-ated. This protocol could be performed without using any noble metal catalyst, inert atmosphere, dry sol-vent, and water scavenger.CO 2023 Elsevier Ltd. All rights reserved. |
| WOS关键词 | TERTIARY AMIDES ; HYDROBORATION REDUCTION ; CATALYTIC-HYDROGENATION ; KETONES ; ALDEHYDES ; SECONDARY |
| 资助项目 | West Anhui University[WGKQ2022079] ; West Anhui University[WXZR201935] ; Traditional Chinese Medicine Institute of Anhui Dabie Mountain[TCMADM-2023-14] ; University Research Project of Anhui Province[2022AH051682] ; Postdoctoral Science Foundation of Anhui Province[2020B454] |
| WOS研究方向 | Chemistry |
| 语种 | 英语 |
| WOS记录号 | WOS:001028869500001 |
| 出版者 | PERGAMON-ELSEVIER SCIENCE LTD |
| 源URL | [http://119.78.100.183/handle/2S10ELR8/306758]  |
| 专题 | 中国科学院上海药物研究所 |
| 通讯作者 | Zang, Yongjun |
| 作者单位 | 1.West Anhui Univ, Tradit Chinese Med Inst Anhui Dabie Mt, Dept Biol & Pharmaceut Engn, Luan 237012, Anhui, Peoples R China 2.Chinese Acad Sci, Shanghai Inst Mat Med, Shanghai 201203, Peoples R China 3.West Anhui Univ, Luan City 237012, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zang, Yongjun,Sui, Qibang,Xu, Qilin,et al. TiCl4-catalyzed deoxygenative reduction of amides to amines using ammonia borane[J]. TETRAHEDRON LETTERS,2023,124:4. |
| APA | Zang, Yongjun,Sui, Qibang,Xu, Qilin,Ma, Menghua,Li, Guosi,&Zhu, Fucheng.(2023).TiCl4-catalyzed deoxygenative reduction of amides to amines using ammonia borane.TETRAHEDRON LETTERS,124,4. |
| MLA | Zang, Yongjun,et al."TiCl4-catalyzed deoxygenative reduction of amides to amines using ammonia borane".TETRAHEDRON LETTERS 124(2023):4. |
入库方式： OAI收割
来源：上海药物研究所
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