Fingerprint of tablet of Corydalis tuber for alleviating pain by HPLC
文献类型：期刊论文
| 作者 | Zhang, Shaojun2; Ouyang, Fan1; Wang, Changhai2; Gu, Ming1 |
| 刊名 | JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
 |
| 出版日期 | 2008 |
| 卷号 | 31期号:3页码:452-464 |
| 关键词 | image chromatographic fingerprint (ICF) digitized chromatographic fingerprint spectrum (DCFS) tablet of Corydalis tuber for alleviating pain quality control pharmaceutical analysis |
| ISSN号 | 1082-6076 |
| 其他题名 | J. Liq. Chromatogr. Relat. Technol. |
| 中文摘要 | An effective analysis method for tablet of Corydalis tuber for alleviating pain was developed by high performance liquid chromatography in the presence of solvent mixtures of acetic acid, triethylamine, methanol, and water in gradient elution. It was applied to 12 tablet samples that were collected stochastically from pharmacies and hospitals. An image chromatographic fingerprint was developed and four marker compounds were identified in the fingerprint. A digitized chromatographic fingerprint spectrum was developed based on the seventeen common peaks that were obtained in these samples. Several quantitative parameters including relative retention time, relative standard deviation of relative retention time, relative peak area, relative standard deviation of relative peak area, difference rate, and total difference rate were applied in the digitized fingerprint of tablet of Corydalis tuberfor alleviating pain to supply an applicable and quantitative quality control method for this kind of traditional Chinese medicine preparation. |
| 英文摘要 | An effective analysis method for tablet of Corydalis tuber for alleviating pain was developed by high performance liquid chromatography in the presence of solvent mixtures of acetic acid, triethylamine, methanol, and water in gradient elution. It was applied to 12 tablet samples that were collected stochastically from pharmacies and hospitals. An image chromatographic fingerprint was developed and four marker compounds were identified in the fingerprint. A digitized chromatographic fingerprint spectrum was developed based on the seventeen common peaks that were obtained in these samples. Several quantitative parameters including relative retention time, relative standard deviation of relative retention time, relative peak area, relative standard deviation of relative peak area, difference rate, and total difference rate were applied in the digitized fingerprint of tablet of Corydalis tuberfor alleviating pain to supply an applicable and quantitative quality control method for this kind of traditional Chinese medicine preparation. |
| WOS标题词 | Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences |
| 类目[WOS] | Biochemical Research Methods ; Chemistry, Analytical |
| 研究领域[WOS] | Biochemistry & Molecular Biology ; Chemistry |
| 关键词[WOS] | PERFORMANCE LIQUID-CHROMATOGRAPHY ; COUNTER-CURRENT CHROMATOGRAPHY ; DL-TETRAHYDROPALMATINE ; INJECTION |
| 收录类别 | SCI |
| 原文出处 | |
| 语种 | 英语 |
| WOS记录号 | WOS:000252348000011 |
| 公开日期 | 2013-10-08 |
| 版本 | 出版稿 |
| 源URL | [http://ir.ipe.ac.cn/handle/122111/2916]  |
| 专题 | 过程工程研究所_研究所（批量导入） |
| 作者单位 | 1.Chinese Acad Sci, Inst Proc Engn, Natl Key Lab Biochem Engn, Beijing 100080, Peoples R China 2.Dalian Univ Technol, Sch Environm & Biol Sci & Technol, Dalian, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhang, Shaojun,Ouyang, Fan,Wang, Changhai,et al. Fingerprint of tablet of Corydalis tuber for alleviating pain by HPLC[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,2008,31(3):452-464. |
| APA | Zhang, Shaojun,Ouyang, Fan,Wang, Changhai,&Gu, Ming.(2008).Fingerprint of tablet of Corydalis tuber for alleviating pain by HPLC.JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,31(3),452-464. |
| MLA | Zhang, Shaojun,et al."Fingerprint of tablet of Corydalis tuber for alleviating pain by HPLC".JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES 31.3(2008):452-464. |
入库方式： OAI收割
来源：过程工程研究所
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