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Nickel coating on hexagonal boron nitride particles by chemical plating

文献类型:期刊论文

作者Li, Fan; Zhang, Dengjun
刊名METALLURGICAL AND MATERIALS TRANSACTIONS B-PROCESS METALLURGY AND MATERIALS PROCESSING SCIENCE
出版日期2007-04-01
卷号38期号:2页码:149-157
ISSN号1073-5615
其他题名Metall. Mater. Trans. B-Proc. Metall. Mater. Proc. Sci.
中文摘要In the present work, a new method was developed to produce nickel-coated boron nitride particles, which could be used as a raw material for making abradable seal layer in gas turbine. Hydrazine was employed as the reducing agent, ammonia solution as the complexing agent, nickel sulfate as the main salt, and ammonia-ammonium sulfate as the buffer system. Thermodynamic consideration showed that the hydrazine reduction could take place in the ammonia-ammonium Sulfate system. The applicability of the ammonia-ammonium sulfate system was further confirmed by experiments. Scanning electron microscopy (SEM) and energy-dispersive spectroscopy (EDS) analyses showed that the coated nickel layer was dense without microcracks. The suitable operation conditions were found to be (1) temperature = 343 to 353 K, (2) [Ni](2+) 0.1 to 0.2 mol/L, (3) concentration of ammonia = 90 to 100 mL/L, (4) mass ratio of Ni2+/BN - 1/3, and (5) mole fraction ratio of hydrazine/Ni2+ = 2. The system was found to be more stable in comparison with the sulfate-tartrate system.
英文摘要In the present work, a new method was developed to produce nickel-coated boron nitride particles, which could be used as a raw material for making abradable seal layer in gas turbine. Hydrazine was employed as the reducing agent, ammonia solution as the complexing agent, nickel sulfate as the main salt, and ammonia-ammonium sulfate as the buffer system. Thermodynamic consideration showed that the hydrazine reduction could take place in the ammonia-ammonium Sulfate system. The applicability of the ammonia-ammonium sulfate system was further confirmed by experiments. Scanning electron microscopy (SEM) and energy-dispersive spectroscopy (EDS) analyses showed that the coated nickel layer was dense without microcracks. The suitable operation conditions were found to be (1) temperature = 343 to 353 K, (2) [Ni](2+) 0.1 to 0.2 mol/L, (3) concentration of ammonia = 90 to 100 mL/L, (4) mass ratio of Ni2+/BN - 1/3, and (5) mole fraction ratio of hydrazine/Ni2+ = 2. The system was found to be more stable in comparison with the sulfate-tartrate system.
WOS标题词Science & Technology ; Technology
类目[WOS]Materials Science, Multidisciplinary ; Metallurgy & Metallurgical Engineering
研究领域[WOS]Materials Science ; Metallurgy & Metallurgical Engineering
收录类别SCI
原文出处://WOS:000247008600001
语种英语
WOS记录号WOS:000247008600001
公开日期2013-10-15
版本出版稿
源URL[http://ir.ipe.ac.cn/handle/122111/3367]  
专题过程工程研究所_研究所(批量导入)
作者单位1.Royal Inst Technol, Dept Mat Sci & Engn, S-10044 Stockholm, Sweden
2.Chinese Acad Sci, Inst Proc Engn, Beijing 100080, Peoples R China
推荐引用方式
GB/T 7714
Li, Fan,Zhang, Dengjun. Nickel coating on hexagonal boron nitride particles by chemical plating[J]. METALLURGICAL AND MATERIALS TRANSACTIONS B-PROCESS METALLURGY AND MATERIALS PROCESSING SCIENCE,2007,38(2):149-157.
APA Li, Fan,&Zhang, Dengjun.(2007).Nickel coating on hexagonal boron nitride particles by chemical plating.METALLURGICAL AND MATERIALS TRANSACTIONS B-PROCESS METALLURGY AND MATERIALS PROCESSING SCIENCE,38(2),149-157.
MLA Li, Fan,et al."Nickel coating on hexagonal boron nitride particles by chemical plating".METALLURGICAL AND MATERIALS TRANSACTIONS B-PROCESS METALLURGY AND MATERIALS PROCESSING SCIENCE 38.2(2007):149-157.

入库方式: OAI收割

来源:过程工程研究所

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