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作者 | Huang, Chao1,2; Wang, Hao1,2; Shi, Wenbei1,2; Sun, Jinfeng4; Hu, Fangyang2,3; Xu, Lei1,2; Yang, Yueheng1,2; Wu, Shitou1,2; Xie, Liewen1,2; Yang, Jinhui1,2
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刊名 | SCIENCE CHINA-EARTH SCIENCES
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出版日期 | 2023-10-12
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页码 | 19 |
ISSN号 | 1674-7313
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关键词 | Mica
In situ analysis by laser ablation
Rb-Sr dating
Triple quadrupole mass spectrometer
Matrix effect
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DOI | 10.1007/s11430-022-1138-4
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英文摘要 | Mica exhibits a relatively high Rb/Sr ratio and possesses a closure temperature for the Rb-Sr isotope system that is higher than the ore-forming temperature range of low- to medium-temperature deposits. Consequently, utilizing the laser ablation (LA) technique for in situ Rb-Sr dating in mica constitutes a significant methodology for resolving the mineralization chronology of low- to medium-temperature hydrothermal ore deposits. In this study, we employed a combination of a triple quadrupole inductively coupled plasma mass spectrometer (ICP-MS/MS) and 193 nm LA system with SF6 as the reaction gas to achieve interference removal of Rb-87(+) on Sr-87(+). We then developed an in situ Rb-Sr dating method for mica. In addition, an investigation was conducted to identify the factors that could influence the analytical accuracy of the method. Subsequently, we applied the developed method to carry out in situ Rb-Sr dating for the ZBH-25 biotite, a national primary reference material (GBW04439) for K-Ar dating, and yielded a younger age (ca. 12%, relative standard deviation, RSD) than the reference K-Ar age when using NIST SRM 610 as the reference material for external calibration. This finding indicated that in the process of determining Rb-Sr ages for mica by LA-ICP-MS/MS, there are significant matrix effects between the NIST SRM 610 and the mica samples, resulting in inaccurate Rb-Sr ages. In response to this issue, a two-step calibration method is proposed here. Based on external calibration using NIST SRM 610, ZBH-25 biotite is employed as a second external reference material to perform a second calibration of the sample data to correct the matrix effect between the glass standards and the natural mica samples, thereby improving the accuracy of Rb-Sr dating by LA-ICP-MS/MS. Using the proposed method, in situ Rb-Sr dating by LA-ICP-MS/MS was performed on mica samples from monzonite exposed in Mt. Dromedary, New South Wales, Australia, porphyritic granodiorite in Fangshan pluton and albionite granite in the Gyirong area of Tibet. The obtained Rb-Sr age results show agreement with the recommended values within the analytical uncertainty, which serves to validate the accuracy and effectiveness of the proposed method. |
WOS关键词 | HIGH-PRECISION ANALYSIS
; ISOTOPIC COMPOSITION
; CHEMICAL-SEPARATION
; SM-ND
; LASER
; AGE
; MS
; STRONTIUM
; SYSTEM
; DISEQUILIBRIUM
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资助项目 | Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China[42173035]
; National Natural Science Foundation of China
; Chinese Academy of Sciences "Key Technology Talent" Project
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WOS研究方向 | Geology
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语种 | 英语
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出版者 | SCIENCE PRESS
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WOS记录号 | WOS:001083269000001
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资助机构 | Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; National Natural Science Foundation of China
; National Natural Science Foundation of China
; National Natural Science Foundation of China
; National Natural Science Foundation of China
; Chinese Academy of Sciences "Key Technology Talent" Project
; Chinese Academy of Sciences "Key Technology Talent" Project
; Chinese Academy of Sciences "Key Technology Talent" Project
; Chinese Academy of Sciences "Key Technology Talent" Project
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; National Natural Science Foundation of China
; National Natural Science Foundation of China
; National Natural Science Foundation of China
; National Natural Science Foundation of China
; Chinese Academy of Sciences "Key Technology Talent" Project
; Chinese Academy of Sciences "Key Technology Talent" Project
; Chinese Academy of Sciences "Key Technology Talent" Project
; Chinese Academy of Sciences "Key Technology Talent" Project
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; National Natural Science Foundation of China
; National Natural Science Foundation of China
; National Natural Science Foundation of China
; National Natural Science Foundation of China
; Chinese Academy of Sciences "Key Technology Talent" Project
; Chinese Academy of Sciences "Key Technology Talent" Project
; Chinese Academy of Sciences "Key Technology Talent" Project
; Chinese Academy of Sciences "Key Technology Talent" Project
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; Acknowledgements The authors express gratitude to the responsible editor and three anonymous reviewers for their valuable comments and suggestions on this manuscript. This work was supported by the National Natural Science Foundation of China
; National Natural Science Foundation of China
; National Natural Science Foundation of China
; National Natural Science Foundation of China
; National Natural Science Foundation of China
; Chinese Academy of Sciences "Key Technology Talent" Project
; Chinese Academy of Sciences "Key Technology Talent" Project
; Chinese Academy of Sciences "Key Technology Talent" Project
; Chinese Academy of Sciences "Key Technology Talent" Project
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源URL | [http://ir.iggcas.ac.cn/handle/132A11/110740] |
专题 | 地质与地球物理研究所_岩石圈演化国家重点实验室 地质与地球物理研究所_中国科学院矿产资源研究重点实验室
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通讯作者 | Huang, Chao |
作者单位 | 1.Chinese Acad Sci, Inst Geol & Geophys, State Key Lab Lithospher Evolut, Beijing 100029, Peoples R China 2.Chinese Acad Sci, Innovat Acad Earth Sci, Beijing 100029, Peoples R China 3.Chinese Acad Sci, Inst Geol & Geophys, Key Lab Mineral Resources, Beijing 100029, Peoples R China 4.Univ Chinese Acad Sci, Coll Earth & Planetary Sci, Beijing 100049, Peoples R China
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推荐引用方式 GB/T 7714 |
Huang, Chao,Wang, Hao,Shi, Wenbei,et al. In situ Rb-Sr dating of mica by LA-ICP-MS/MS[J]. SCIENCE CHINA-EARTH SCIENCES,2023:19.
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APA |
Huang, Chao.,Wang, Hao.,Shi, Wenbei.,Sun, Jinfeng.,Hu, Fangyang.,...&Yang, Jinhui.(2023).In situ Rb-Sr dating of mica by LA-ICP-MS/MS.SCIENCE CHINA-EARTH SCIENCES,19.
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MLA |
Huang, Chao,et al."In situ Rb-Sr dating of mica by LA-ICP-MS/MS".SCIENCE CHINA-EARTH SCIENCES (2023):19.
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