Design and Synthesis of Fluorine-Containing Embedded Carbon Dots Stationary Phase for Separation of Versatile Analytes
文献类型：期刊论文
| 作者 | Song, Zhihua3; Wu, Wenpu3; Sui, Lei3; Han, Xinyan3; Xu, Hui3; Yang, Gangqiang3; Zhang, Peng3; Zhou, Na2; Chen, Lingxin1,2 ; Li, Jinhua2
|
| 刊名 | ANALYTICAL CHEMISTRY
 |
| 出版日期 | 2024-10-04 |
| 卷号 | 96期号:42页码:16590-16598 |
| ISSN号 | 0003-2700 |
| DOI | 10.1021/acs.analchem.4c02411 |
| 通讯作者 | Song, Zhihua(zhihuasong08@yeah.net) ; Li, Jinhua(jhli@yic.ac.cn) |
| 英文摘要 | Thus far, numerous new stationary phases have been developed. A fluorine-containing embedded carbon dots (F3-CDs-SiO2) stationary phase was first designed and synthesized. The resulting F3-CDs-SiO2 stationary phase was characterized carefully by scanning electron microscopy, transmission electron microscopy, elemental analysis, X-ray photoelectron spectroscopy, and Brunauer-Emmett-Teller experiment. The F3-CDs-SiO2 stationary phase was slurry packed into the HPLC column (150 x 2.1 mm) for evaluation. Furthermore, the F3-CDs-SiO2 column was successfully used for separation of pesticides, nucleosides, sulfonamides, alkaloids, and alkylbenzenes. The retention mechanism (including hydrophobic interaction, F-F, hydrogen bond interaction, ion-exchange, dipole-dipole interaction, electrostatic interaction, etc.) was investigated carefully. Meanwhile, the F3-SiO2 stationary phase was synthesized and used to evaluate the role of CDs. Furthermore, various commercial stationary phases (including amino-SiO2, diol-SiO2, C18-SiO2, and PFP-SiO2) were used for comparison. Moreover, the F3-CDs-SiO2 column possessed good repeatability, reproducibility, and stability in separation of versatile analytes. |
| WOS关键词 | LIQUID-CHROMATOGRAPHY ; SILICA |
| WOS研究方向 | Chemistry |
| 语种 | 英语 |
| WOS记录号 | WOS:001330129700001 |
| 资助机构 | National Natural Science Foundation of China ; Shandong Provincial Natural Science Foundation ; Project of Yantai Growth Drivers Conversion Research Institute ; Yantai Science and Technology Achievement Transfer and Transformation Demonstration Base ; Youth Innovation Team Plan of Shandong Province |
| 源URL | [http://ir.yic.ac.cn/handle/133337/37132]  |
| 专题 | 烟台海岸带研究所_中科院海岸带环境过程与生态修复重点实验室 烟台海岸带研究所_山东省海岸带环境工程技术研究中心 支撑部门_所级公共技术服务中心 |
| 通讯作者 | Song, Zhihua; Li, Jinhua |
| 作者单位 | 1.Binzhou Med Univ, Sch Pharm, Yantai 264003, Peoples R China 2.Chinese Acad Sci, Yantai Inst Coastal Zone Res, Res Ctr Coastal Environm Engn & Technol, CAS Key Lab Coastal Environm Proc & Ecol Remediat, Yantai 264003, Peoples R China 3.Yantai Univ, Sch Pharm, Collaborat Innovat Ctr Adv Drug Delivery Syst & Bi, Key Lab Mol Pharmacol & Drug Evaluat,Minist Educ, Yantai 264005, Peoples R China |
| 推荐引用方式 GB/T 7714 | Song, Zhihua,Wu, Wenpu,Sui, Lei,et al. Design and Synthesis of Fluorine-Containing Embedded Carbon Dots Stationary Phase for Separation of Versatile Analytes[J]. ANALYTICAL CHEMISTRY,2024,96(42):16590-16598. |
| APA | Song, Zhihua.,Wu, Wenpu.,Sui, Lei.,Han, Xinyan.,Xu, Hui.,...&Li, Jinhua.(2024).Design and Synthesis of Fluorine-Containing Embedded Carbon Dots Stationary Phase for Separation of Versatile Analytes.ANALYTICAL CHEMISTRY,96(42),16590-16598. |
| MLA | Song, Zhihua,et al."Design and Synthesis of Fluorine-Containing Embedded Carbon Dots Stationary Phase for Separation of Versatile Analytes".ANALYTICAL CHEMISTRY 96.42(2024):16590-16598. |
入库方式： OAI收割
来源：烟台海岸带研究所
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。