The Suppression Method of Raman Laser Thermal Effect for Sensitive Samples
文献类型：期刊论文
| 作者 | Chen, Pei-li1; Song, Da1,2; Zhou, Zhao-qiu1; Chen, Kai-yue1; Su, Qiu-cheng1; Li, Cui-qin3 |
| 刊名 | SPECTROSCOPY AND SPECTRAL ANALYSIS
 |
| 出版日期 | 2024-09-01 |
| 卷号 | 44期号:9页码:2476-2481 |
| 关键词 | Nondestructive characterizations Carbon structure parameters Raman spectroscopy |
| ISSN号 | 1000-0593 |
| DOI | 10.3964/j.issn.1000-0593(2024)09-2476-06 |
| 通讯作者 | Li, Cui-qin(dqpilicuiqin@126.com) |
| 英文摘要 | Laser-micro confocal Raman spectroscopy is widely used to study molecular structure, bonding effects. loading, and bternal stress. The signal intensity and quality of Raman spectra are particularly important for the analysis. However. Raman Maser irradiation the surface of sensitive samples produces thermal effects and, thus structural damage. The damaged parts of the sample collapse and shine. To obtain high quality Raman spectra and realize non destructive characterization, this paper novatively proposes adding KBr as heat sink to climinate the thermal effect of laser. A series of carbon materials that are Jasily damaged under laser radiation were selected as the research objects and the relationships between the carbon content of the samples, the addition of KBr. and the Raman spectral parameters and signal intensity were explored, The experimental Fesults show that adding KBr can effectively inhibit the sensitive samples from being damaged by the Raman laser. When the ddition ratio of KBr is 12. accurate and nondestructive Raman spectroscopic detection of this material can be realized. In Addition, the graphitization R values of carbon materials detected in different microregions are very close to each other, with the nerease of carbon content, the position of the D peak is shifted to the low-wave region by 3 cm(-1) and the position of the G peak in shifted to the high wave region by 2 cm(-1) increased with a decrease the intensity ratio and the difference between the peak positions of the D peak and the G peak and an increase in the ordering of the samples. |
| WOS关键词 | SPECTROSCOPY |
| WOS研究方向 | Spectroscopy |
| 语种 | 英语 |
| WOS记录号 | WOS:001316649500001 |
| 出版者 | OFFICE SPECTROSCOPY & SPECTRAL ANALYSIS |
| 源URL | [http://ir.giec.ac.cn/handle/344007/42942]  |
| 专题 | 中国科学院广州能源研究所 |
| 通讯作者 | Li, Cui-qin |
| 作者单位 | 1.Guangzhou Inst Energy Convers, Chinese Acad Sci, Guangzhou 510640, Peoples R China 2.Univ Sci & Technol China, Hefei 230026, Peoples R China 3.Northeast Petr Univ, Daqing 163319, Peoples R China |
| 推荐引用方式 GB/T 7714 | Chen, Pei-li,Song, Da,Zhou, Zhao-qiu,et al. The Suppression Method of Raman Laser Thermal Effect for Sensitive Samples[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS,2024,44(9):2476-2481. |
| APA | Chen, Pei-li,Song, Da,Zhou, Zhao-qiu,Chen, Kai-yue,Su, Qiu-cheng,&Li, Cui-qin.(2024).The Suppression Method of Raman Laser Thermal Effect for Sensitive Samples.SPECTROSCOPY AND SPECTRAL ANALYSIS,44(9),2476-2481. |
| MLA | Chen, Pei-li,et al."The Suppression Method of Raman Laser Thermal Effect for Sensitive Samples".SPECTROSCOPY AND SPECTRAL ANALYSIS 44.9(2024):2476-2481. |
入库方式： OAI收割
来源：广州能源研究所
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