SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY
文献类型：期刊论文
| 作者 | Yang Yi; Bakri Mahinur; Gu Dongyu; Aisa Haji Akber
|
| 刊名 | JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
 |
| 出版日期 | 2013 |
| 卷号 | 36期号:5页码:573-582 |
| 关键词 | bioactive compound (S)-dehydrovomifoliol high-speed counter-current chromatography Nitraria sibirica Pall separation traditional Uighur Medicine |
| ISSN号 | 1082-6076 |
| 通讯作者 | Aisa, HA |
| 中文摘要 | An effective high-speed countercurrent chromatography (HSCCC) method was established for separation and purification of (S)-dehydrovomifoliol from the leaves of Nitraria sibirica Pall. (NS). HSCCC was performed with a two-phase solvent systems composed of n-hexane-ethyl acetate-methanol-water (1:5:1:5, v/v) at a flow rate of 2mL/min. From 1g crude sample of NS, 23mg (S)-dehydrovomifoliol was obtained at purity of 95%. The chemical structure was confirmed by MS, 1H NMR, and 13C NMR. (S)-dehydrovomifoliol was isolated from Nitraria genus for the first time. |
| 学科主题 | Biochemistry & Molecular Biology ; Chemistry |
| 收录类别 | SCI |
| 资助信息 | West Light Foundation of The Chinese Academy of Sciences XBBS201011; China National Funds for Distinguished Young Scientists 30925045 |
| 公开日期 | 2013-11-07 |
| 源URL | [http://ir.xjipc.cas.cn/handle/365002/2685]  |
| 专题 | 新疆理化技术研究所_省部共建新疆特有药用资源利用重点实验室 新疆理化技术研究所_资源化学研究室 |
| 作者单位 | Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Key Lab Xinjiang Indigenous Med Plants Resource U, Urumqi 830011, Peoples R China;Chinese Acad Sci, Grad Univ, Beijing, Peoples R China |
| 推荐引用方式 GB/T 7714 | Yang Yi,Bakri Mahinur,Gu Dongyu,et al. SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,2013,36(5):573-582. |
| APA | Yang Yi,Bakri Mahinur,Gu Dongyu,&Aisa Haji Akber.(2013).SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY.JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,36(5),573-582. |
| MLA | Yang Yi,et al."SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY".JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES 36.5(2013):573-582. |
入库方式： OAI收割
来源：新疆理化技术研究所
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