Preparation of Anhydrous Magnesium Chloride from Magnesia
文献类型：期刊论文
| 作者 | Zhang, Zhimin1,2; Lu, Xuchen1,3; Yang, Suping1,2; Pan, Feng1,2
|
| 刊名 | INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH
 |
| 出版日期 | 2012-07-25 |
| 卷号 | 51期号:29页码:9713-9718 |
| 关键词 | THERMAL-DECOMPOSITION |
| ISSN号 | 0888-5885 |
| 通讯作者 | Lu, XC |
| 英文摘要 | High-purity anhydrous magnesium chloride was prepared by using magnesia and ammonium chloride as reactants, alumina as covering agent. The process was characterized by X-ray diffraction and thermogravimetric and differential scanning calorimetry analysis. The reaction mechanism involved in the process was proposed and discussed. In addition, the effects of molar ratio of ammonium chloride to magnesia, thickness of the covering agent (alumina), reaction temperature, and reaction time on the purity of anhydrous magnesium chloride were investigated. The content of magnesia in anhydrous magnesium chloride was achieved 0.014% under the optimum conditions: ammonium chloride and magnesia with the molar ratio of NH4Cl:MgO = 5:1 were mixed evenly. Alumina with the thickness of 1.1 cm was used as a covering agent. The mixture was maintained at 450 degrees C for 1.5 h for the complete reaction, and then calcined at 700 degrees C for 0.5 h to obtain well-sintered anhydrous magnesium chloride. |
| WOS标题词 | Science & Technology ; Technology |
| 类目[WOS] | Engineering, Chemical |
| 研究领域[WOS] | Engineering |
| 关键词[WOS] | THERMAL-DECOMPOSITION |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000306725400002 |
| 公开日期 | 2013-10-16 |
| 版本 | 出版稿 |
| 源URL | [http://ir.ipe.ac.cn/handle/122111/3552]  |
| 专题 | 过程工程研究所_多相复杂系统国家重点实验室 |
| 作者单位 | 1.Chinese Acad Sci, Inst Proc Engn, State Key Lab Multiphase Complex Syst, Beijing 100190, Peoples R China 2.Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China 3.United Res Ctr Resource & Mat, Wuhai 016000, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhang, Zhimin,Lu, Xuchen,Yang, Suping,et al. Preparation of Anhydrous Magnesium Chloride from Magnesia[J]. INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH,2012,51(29):9713-9718. |
| APA | Zhang, Zhimin,Lu, Xuchen,Yang, Suping,&Pan, Feng.(2012).Preparation of Anhydrous Magnesium Chloride from Magnesia.INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH,51(29),9713-9718. |
| MLA | Zhang, Zhimin,et al."Preparation of Anhydrous Magnesium Chloride from Magnesia".INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH 51.29(2012):9713-9718. |
入库方式： OAI收割
来源：过程工程研究所
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