Separation and purification of Z ligustilide and senkyunolide A from Ligusticum chuanxiong Hort. with supercritical fluid extraction and high-speed counter-current chromatography
文献类型：期刊论文
| 作者 | Zhang, Dalei; Teng, Houlei; Li, Guisheng; Liu, Ke; Su, Zhiguo |
| 刊名 | SEPARATION SCIENCE AND TECHNOLOGY
 |
| 出版日期 | 2006 |
| 卷号 | 41期号:15页码:3397-3408 |
| 关键词 | counter-current chromatography Z ligustilide senkyunolide A Ligusticum chuanxiong |
| ISSN号 | 0149-6395 |
| 其他题名 | Sep. Sci. Technol. |
| 中文摘要 | The essential oil was obtained by supercritical fluid extraction from dried roots of Ligusticum chuanxiong. Different solvent systems for high-speed counter-current chromatography (HSCCC) were compared. A system composed of n hexane-ethyl acetate-methanol-water-acetonitrile in the ratio of 8:2:5:5:3 (v/v) was found to be optimum for HSCCC of the essential oil. Z ligustilide and senkyunolide A were separated by HSCCC with purity of 98% determined by GC. The chemical structures of these two components were identified by nuclear magnetic resonance (NMR) and mass spectrometry (MS). |
| 英文摘要 | The essential oil was obtained by supercritical fluid extraction from dried roots of Ligusticum chuanxiong. Different solvent systems for high-speed counter-current chromatography (HSCCC) were compared. A system composed of n hexane-ethyl acetate-methanol-water-acetonitrile in the ratio of 8:2:5:5:3 (v/v) was found to be optimum for HSCCC of the essential oil. Z ligustilide and senkyunolide A were separated by HSCCC with purity of 98% determined by GC. The chemical structures of these two components were identified by nuclear magnetic resonance (NMR) and mass spectrometry (MS). |
| WOS标题词 | Science & Technology ; Physical Sciences ; Technology |
| 类目[WOS] | Chemistry, Multidisciplinary ; Engineering, Chemical |
| 研究领域[WOS] | Chemistry ; Engineering |
| 关键词[WOS] | PREPARATIVE SEPARATION ; CHINESE ; TEA |
| 收录类别 | SCI |
| 原文出处 | |
| 语种 | 英语 |
| WOS记录号 | WOS:000241680900007 |
| 公开日期 | 2013-10-24 |
| 版本 | 出版稿 |
| 源URL | [http://ir.ipe.ac.cn/handle/122111/4067]  |
| 专题 | 过程工程研究所_研究所（批量导入） |
| 作者单位 | 1.Chinese Acad Sci, Inst Proc Engn, Natl Key Lab Biochem Engn, Beijing 100080, Peoples R China 2.Yantai Univ, Sch Pharm, Shandong, Peoples R China 3.Shandong Engn Res Ctr Nat Drugs, Shandong, Peoples R China 4.Chinese Acad Sci, Grad Sch, Beijing 100080, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhang, Dalei,Teng, Houlei,Li, Guisheng,et al. Separation and purification of Z ligustilide and senkyunolide A from Ligusticum chuanxiong Hort. with supercritical fluid extraction and high-speed counter-current chromatography[J]. SEPARATION SCIENCE AND TECHNOLOGY,2006,41(15):3397-3408. |
| APA | Zhang, Dalei,Teng, Houlei,Li, Guisheng,Liu, Ke,&Su, Zhiguo.(2006).Separation and purification of Z ligustilide and senkyunolide A from Ligusticum chuanxiong Hort. with supercritical fluid extraction and high-speed counter-current chromatography.SEPARATION SCIENCE AND TECHNOLOGY,41(15),3397-3408. |
| MLA | Zhang, Dalei,et al."Separation and purification of Z ligustilide and senkyunolide A from Ligusticum chuanxiong Hort. with supercritical fluid extraction and high-speed counter-current chromatography".SEPARATION SCIENCE AND TECHNOLOGY 41.15(2006):3397-3408. |
入库方式： OAI收割
来源：过程工程研究所
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