Template-free synthesis of NiO hollow microspheres covered with nanoflakes
文献类型：期刊论文
| 作者 | Liu, Jian; Du, Shangfeng; Wei, Lianqi; Liu, Haidi; Tian, Yajun; Chen, Yunfa
|
| 刊名 | MATERIALS LETTERS
 |
| 出版日期 | 2006-12-01 |
| 卷号 | 60期号:29-30页码:3601-3604 |
| 关键词 | NiO solvothermal nanomaterials microstructure hollow microspheres |
| ISSN号 | 0167-577X |
| 其他题名 | Mater. Lett. |
| 中文摘要 | alpha-Ni(OH)(2) hollow microspheres precursors were synthesized without any template through a solvothermal method. Hydrolyzing NiCl2 in alkaline solution, the Ni(OH)(2) hollow microspheres covered with a disordered covering of perpendicular nanoflakes were prepared. Subsequently, the similar microstructured NiO hollow microspheres with BET area around 222.8 m(2)/g and specific pore volume around 0.5 cm(3)/g were obtained by calcining the above precursor at 250-300 degrees C with a slow heating rate (about 1 K/min). The effects of the surfactant and the calcining temperature on the morphology and the mesostructure of the NiO hollow microspheres were also discussed. (c) 2006 Elsevier B.V. All rights reserved. |
| 英文摘要 | alpha-Ni(OH)(2) hollow microspheres precursors were synthesized without any template through a solvothermal method. Hydrolyzing NiCl2 in alkaline solution, the Ni(OH)(2) hollow microspheres covered with a disordered covering of perpendicular nanoflakes were prepared. Subsequently, the similar microstructured NiO hollow microspheres with BET area around 222.8 m(2)/g and specific pore volume around 0.5 cm(3)/g were obtained by calcining the above precursor at 250-300 degrees C with a slow heating rate (about 1 K/min). The effects of the surfactant and the calcining temperature on the morphology and the mesostructure of the NiO hollow microspheres were also discussed. (c) 2006 Elsevier B.V. All rights reserved. |
| WOS标题词 | Science & Technology ; Technology ; Physical Sciences |
| 类目[WOS] | Materials Science, Multidisciplinary ; Physics, Applied |
| 研究领域[WOS] | Materials Science ; Physics |
| 关键词[WOS] | NICKEL-OXIDE ; FABRICATION ; SPHERES ; HYDROXIDE |
| 收录类别 | SCI |
| 原文出处 | |
| 语种 | 英语 |
| WOS记录号 | WOS:000242469000038 |
| 公开日期 | 2013-10-24 |
| 版本 | 出版稿 |
| 源URL | [http://ir.ipe.ac.cn/handle/122111/4102]  |
| 专题 | 过程工程研究所_研究所（批量导入） |
| 作者单位 | 1.Chinese Acad Sci, Inst Proc Engn, Key Lab Multi Phase React, Beijing 100080, Peoples R China 2.Grad Univ, Chinese Acad Sci, Dept Chem & Chem Engn, Beijing 100039, Peoples R China |
| 推荐引用方式 GB/T 7714 | Liu, Jian,Du, Shangfeng,Wei, Lianqi,et al. Template-free synthesis of NiO hollow microspheres covered with nanoflakes[J]. MATERIALS LETTERS,2006,60(29-30):3601-3604. |
| APA | Liu, Jian,Du, Shangfeng,Wei, Lianqi,Liu, Haidi,Tian, Yajun,&Chen, Yunfa.(2006).Template-free synthesis of NiO hollow microspheres covered with nanoflakes.MATERIALS LETTERS,60(29-30),3601-3604. |
| MLA | Liu, Jian,et al."Template-free synthesis of NiO hollow microspheres covered with nanoflakes".MATERIALS LETTERS 60.29-30(2006):3601-3604. |
入库方式： OAI收割
来源：过程工程研究所
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