Processing and microstructure of LaCrO3 thin film derived from chelating precursors
文献类型:期刊论文
作者 | Lu, XC; Xu, TX; Dong, XH |
刊名 | JOURNAL OF RARE EARTHS
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出版日期 | 2000-09-01 |
卷号 | 18期号:3页码:196-200 |
关键词 | rare earths thin film deposition process organic chelate lanthanum orthochromite |
ISSN号 | 1002-0721 |
其他题名 | J. Rare Earths |
中文摘要 | LaCrO3 thin films were successfully prepared at lower temperatures by the sol-gel process based on organic chelating precursors. The formation and transition of the gel derived from the chelate solution were analyzed by means of IR, DTA-TG, XRD and TEM. In addition, the formation and microstructure of thin films were investigated by SEM and XRD. The results show that the gel formed by the condensation reaction is decomposed at about 195 degrees C, transformed into a great quantity of LaCrO3 by heat-treating at 200 degrees C for 1 h, and the complexing ways in the gel have an important influence upon the formation of LaCrO3. The formation process of thin film includes the nucleation and growth on the substrate, the formation of polycrystalline islands and the continuous film by repeating the dip-coating process. Higher heat-treatment temperature gives rise to larger granules in the thin film. |
英文摘要 | LaCrO3 thin films were successfully prepared at lower temperatures by the sol-gel process based on organic chelating precursors. The formation and transition of the gel derived from the chelate solution were analyzed by means of IR, DTA-TG, XRD and TEM. In addition, the formation and microstructure of thin films were investigated by SEM and XRD. The results show that the gel formed by the condensation reaction is decomposed at about 195 degrees C, transformed into a great quantity of LaCrO3 by heat-treating at 200 degrees C for 1 h, and the complexing ways in the gel have an important influence upon the formation of LaCrO3. The formation process of thin film includes the nucleation and growth on the substrate, the formation of polycrystalline islands and the continuous film by repeating the dip-coating process. Higher heat-treatment temperature gives rise to larger granules in the thin film. |
WOS标题词 | Science & Technology ; Physical Sciences |
类目[WOS] | Chemistry, Applied |
研究领域[WOS] | Chemistry |
收录类别 | SCI |
原文出处 | |
语种 | 英语 |
WOS记录号 | WOS:000089231300009 |
公开日期 | 2013-11-15 |
版本 | 出版稿 |
源URL | [http://ir.ipe.ac.cn/handle/122111/6032] ![]() |
专题 | 过程工程研究所_研究所(批量导入) |
作者单位 | 1.Chinese Acad Sci, Inst Chem Met, Beijing 100080, Peoples R China 2.Tianjin Univ, Inst Mat Sci & Engn, Tianjin 300072, Peoples R China |
推荐引用方式 GB/T 7714 | Lu, XC,Xu, TX,Dong, XH. Processing and microstructure of LaCrO3 thin film derived from chelating precursors[J]. JOURNAL OF RARE EARTHS,2000,18(3):196-200. |
APA | Lu, XC,Xu, TX,&Dong, XH.(2000).Processing and microstructure of LaCrO3 thin film derived from chelating precursors.JOURNAL OF RARE EARTHS,18(3),196-200. |
MLA | Lu, XC,et al."Processing and microstructure of LaCrO3 thin film derived from chelating precursors".JOURNAL OF RARE EARTHS 18.3(2000):196-200. |
入库方式: OAI收割
来源:过程工程研究所
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