Synthesis and properties of La0.6Sr0.4CoO3−δ nanopowder
文献类型:期刊论文
作者 | Tao YK ; Shao J ; Wang JX ; Wang WG |
刊名 | Journal of Power Sources
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出版日期 | 2008 |
期号 | 185页码:609–614 |
关键词 | La0.6Sr0.4CoO3−δ Nanopowder Cathode Polarization resistance |
合作状况 | 国内 |
中文摘要 | Uniform nanopowders of La0.6Sr0.4CoO3−ı (LSC)were synthesized by the combined citrate–EDTA method.The precursor solution was prepared from nitrates of the constituent metal ion, citric acid and EDTA with a pH value controlled by ammonia. The obtained product was characterized by TG/DTA, XRD, SEM, and BET measurements. The single perovskite phase could form completely after sintering at the temperature of 900℃. There was no significant effect of the precursor solution pH value on the perovskite phase formation temperature; however, LSC powders prepared from the precursors with different pH values showed specific shapes. The morphology of La0.6Sr0.4CoO3−δ powder was also optimized with proper surfactant addition. The sintered La0.6Sr0.4CoO3−δ bulk samples exhibited an electrical conductivity of 1867Scm−1 in air at 800℃. The impedance spectra of a symmetric LSC cathode on a GDC electrolyte substrate were measured and polarization resistance (Rp) values of 0.17Ωcm2 at 700℃ and 0.07Ωcm2 at 750℃ in air were obtained. |
收录类别 | SCI |
语种 | 英语 |
公开日期 | 2009-12-24 |
源URL | [http://ir.nimte.ac.cn/handle/174433/105] ![]() |
专题 | 宁波材料技术与工程研究所_宁波所知识产出 |
推荐引用方式 GB/T 7714 | Tao YK,Shao J,Wang JX,et al. Synthesis and properties of La0.6Sr0.4CoO3−δ nanopowder[J]. Journal of Power Sources,2008(185):609–614. |
APA | Tao YK,Shao J,Wang JX,&Wang WG.(2008).Synthesis and properties of La0.6Sr0.4CoO3−δ nanopowder.Journal of Power Sources(185),609–614. |
MLA | Tao YK,et al."Synthesis and properties of La0.6Sr0.4CoO3−δ nanopowder".Journal of Power Sources .185(2008):609–614. |
入库方式: OAI收割
来源:宁波材料技术与工程研究所
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