Synthesis and properties of (La0.75Sr0.25)0.95MnO3±δ nano-powder prepared via Pechini route
文献类型:期刊论文
作者 | Wang JX ; Tao YK ; Shao J ; Wang WG |
刊名 | Journal of Power Sources
![]() |
出版日期 | 2009 |
期号 | 186页码:344–348 |
关键词 | Nanocrystalline powders Lanthanum manganate composite cathode Polarization resistance |
合作状况 | 国内 |
中文摘要 | (La0.75Sr0.25)0.95MnO3±δ (LSM) powders have been synthesized via a Pechini route. The prepared powders were characterized by XRD, SEM, XRF, BET and particle size distribution (PSD) analysis. It is shown that the morphology and structure of the oxide particles are significantly dependent on the preparation conditions such as the sort of surfactant andpHvalue of the starting solution. High purity, single phase,homogeneous, nanocrystalline LSMpowders with slight aggregationwere obtained using citric acid as complexing agent, ethylene glycol as surfactant and pH 1. The conductivity of the sintered LSM sample prepared from this nanocrystalline powderswas mensurated about 200 S cm−1 in air at 600–1000 ℃. The impedance spectra of symmetric cells LSM–YSZ/YSZ/LSM–YSZ were measured in air and open circuit voltage condition. The optimal polarization resistance (Rp) of 0.175Ωcm2 at 750℃ and 0.07Ωcm2 at 800℃ was obtained in the sample with LSM to YSZ weight ratio of 49:51. |
收录类别 | SCI |
语种 | 英语 |
公开日期 | 2009-12-24 |
源URL | [http://ir.nimte.ac.cn/handle/174433/106] ![]() |
专题 | 宁波材料技术与工程研究所_宁波所知识产出 |
推荐引用方式 GB/T 7714 | Wang JX,Tao YK,Shao J,et al. Synthesis and properties of (La0.75Sr0.25)0.95MnO3±δ nano-powder prepared via Pechini route[J]. Journal of Power Sources,2009(186):344–348. |
APA | Wang JX,Tao YK,Shao J,&Wang WG.(2009).Synthesis and properties of (La0.75Sr0.25)0.95MnO3±δ nano-powder prepared via Pechini route.Journal of Power Sources(186),344–348. |
MLA | Wang JX,et al."Synthesis and properties of (La0.75Sr0.25)0.95MnO3±δ nano-powder prepared via Pechini route".Journal of Power Sources .186(2009):344–348. |
入库方式: OAI收割
来源:宁波材料技术与工程研究所
浏览0
下载0
收藏0
其他版本
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。