中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Preparation and Characterization of Poly(butylene terephthalate)/Silica Nanocomposites

文献类型:期刊论文

作者Yao XY ; Tian XY ; Zhang X ; Zheng K ; Zheng J ; Wang RX ; Kang SH ; Cui P
刊名POLYMER ENGINEERING AND SCIENCE
出版日期2009
期号49页码:799-807
合作状况国内
中文摘要In this study, we presented a convenient, in situ polymerization route for the preparation of Poly (butylene terephthalate) (PBT)/silica nanocomposites, in which silica was not premodified. The nanocomposites were synthesized by in situ polymerization of terephthalic acid (TPA), 1,4-butanediol (BD) and silica. The structure of these nanocomposites were investigated by Fourier transform infrared (FTIR) and thermogravimetric analyses (TGA). The results show that PBT chains were successfully grafted onto the surface of silica. Transmission electron microscope (TEM) micrographs revealed that silica were homogeneously dispersed in PBT matrix at a size level of 10–20 nm. The isothermal crystallization kinetics of pure PBT and PBT/silica nanocomposites were investigated by differential scanning calorimeter (DSC) and simulated by Avrami model. The existence of silica could lead to an acceleration of crystallization and enhance the thermal stability of PBT. According to dynamic mechanical analysis (DMA), the storage modulus of PBT/silica nanocomposites were markedly improved compared with pure PBT.
收录类别SCI
语种英语
公开日期2010-01-05
源URL[http://ir.nimte.ac.cn/handle/174433/214]  
专题宁波材料技术与工程研究所_宁波所知识产出
推荐引用方式
GB/T 7714
Yao XY,Tian XY,Zhang X,et al. Preparation and Characterization of Poly(butylene terephthalate)/Silica Nanocomposites[J]. POLYMER ENGINEERING AND SCIENCE,2009(49):799-807.
APA Yao XY.,Tian XY.,Zhang X.,Zheng K.,Zheng J.,...&Cui P.(2009).Preparation and Characterization of Poly(butylene terephthalate)/Silica Nanocomposites.POLYMER ENGINEERING AND SCIENCE(49),799-807.
MLA Yao XY,et al."Preparation and Characterization of Poly(butylene terephthalate)/Silica Nanocomposites".POLYMER ENGINEERING AND SCIENCE .49(2009):799-807.

入库方式: OAI收割

来源:宁波材料技术与工程研究所

浏览0
下载0
收藏0
其他版本

除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。