Morphology control of Ce0.9Gd0.1O1.95 nanopowder synthesized by sol–gel method using PVP as a surfactant
文献类型：期刊论文
| 作者 | Tao YK ; Shao J ; Wang JX ; Wang WG |
| 刊名 | Journal of Alloys and Compounds
 |
| 出版日期 | 2009 |
| 期号 | 484页码:729–733 |
| 关键词 | Sol–gel synthesis Chemical synthesis Nanostructures Ionic conduction |
| 合作状况 | 国内 |
| 中文摘要 | In thiswork,well-dispersed nanopowder of Ce0.9Gd0.1O1.95 (gadolinia doped ceria, GDC)was synthesized by a novel sol−gel thermolysis method using a combination of citrate acid and polyvinylpyrrolidone (PVP). PVP performed as a surfactant and its amountwas optimized in terms of GDC powder morphology. The physical and chemical properties of the resultants were characterized by XRD, TG/DTA, FT–IR, SEM, BET and PSA. From the XRD patterns, well-crystalline cubic fluorite structured GDC was obtained after calcining the precursor at 600 ℃. The SEM observation showed an average particle size of about 15nm for the optimal GDC powder and particle size analysis (PSA) gave a narrow distribution of particle size. The sintering experiment showed a good sinterability and a relative density of 94% was achieved at 1300℃. The dense sample exhibited an ionic conductivity of 0.017 S cm−1 at 600 ℃ in air. |
| 收录类别 | SCI |
| 语种 | 英语 |
| 公开日期 | 2010-01-07 |
| 源URL | [http://ir.nimte.ac.cn/handle/174433/246]  |
| 专题 | 宁波材料技术与工程研究所_宁波所知识产出 |
| 推荐引用方式 GB/T 7714 | Tao YK,Shao J,Wang JX,et al. Morphology control of Ce0.9Gd0.1O1.95 nanopowder synthesized by sol–gel method using PVP as a surfactant[J]. Journal of Alloys and Compounds,2009(484):729–733. |
| APA | Tao YK,Shao J,Wang JX,&Wang WG.(2009).Morphology control of Ce0.9Gd0.1O1.95 nanopowder synthesized by sol–gel method using PVP as a surfactant.Journal of Alloys and Compounds(484),729–733. |
| MLA | Tao YK,et al."Morphology control of Ce0.9Gd0.1O1.95 nanopowder synthesized by sol–gel method using PVP as a surfactant".Journal of Alloys and Compounds .484(2009):729–733. |
入库方式： OAI收割
来源：宁波材料技术与工程研究所
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