中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Preparation of Cr2O3 nanoparticles via C2H5OH hydrothermal reduction

文献类型:期刊论文

作者Pei, Zhenzhao1,2; Xu, Hongbin1; Zhang, Yi1
刊名JOURNAL OF ALLOYS AND COMPOUNDS
出版日期2009-01-22
卷号468期号:1-2页码:L5-L8
关键词Nanoparticles Hydrothermal synthesis Cr2O3 Average particle size Specific surface area
ISSN号0925-8388
通讯作者Xu, HB
英文摘要Nanoparticles of chromic oxide (Cr2O3) are widely used in many fields serving as catalysts, wear resistance materials, and advanced colorants. with chromium anhydride (CrO3) and anhydrous alcohol (C2H5OH) as the raw materials, nanoparticles of Cr2O3 were successfully prepared via hydrothermal synthesis. At a reaction temperature as low as 190 C, the redox reaction could lie completed within only 1 h. The process needs no stirrer and surfactant and it was easily controllable. The obtained products were loosely agglomerated Cr2O3 nanoparticle, with an average particle size ranging from 29 nm to 60 nm. Various approaches including XRD, FE-SEM, TG-DSC, and IR were used to investigate(e the intermediate and final products. The findings show that a higher calcination temperature lends to result in a smaller specific surface area and a larger average particle size. and it higher ratio of C2H5OH to Cro(3) always leads to a higher specific surface area and therefore a smaller average particle size of (lie products. Moreover, the agglomeration of nanoparticles weakens with the increase of calcination temperature. As the process is simple and low-cost, it has the potential to lie produced oil a large scale. (c) 2008 Elsevier B.V. All rights reserved.
WOS标题词Science & Technology ; Physical Sciences ; Technology
类目[WOS]Chemistry, Physical ; Materials Science, Multidisciplinary ; Metallurgy & Metallurgical Engineering
研究领域[WOS]Chemistry ; Materials Science ; Metallurgy & Metallurgical Engineering
关键词[WOS]CHROMIUM-OXIDE ; MAGNETIC-PROPERTIES
收录类别SCI
语种英语
WOS记录号WOS:000263080000002
公开日期2013-12-11
版本出版稿
源URL[http://ir.ipe.ac.cn/handle/122111/6758]  
专题过程工程研究所_湿法冶金清洁生产技术国家工程实验室
作者单位1.Chinese Acad Sci, Inst Proc Engn, Beijing 100080, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China
推荐引用方式
GB/T 7714
Pei, Zhenzhao,Xu, Hongbin,Zhang, Yi. Preparation of Cr2O3 nanoparticles via C2H5OH hydrothermal reduction[J]. JOURNAL OF ALLOYS AND COMPOUNDS,2009,468(1-2):L5-L8.
APA Pei, Zhenzhao,Xu, Hongbin,&Zhang, Yi.(2009).Preparation of Cr2O3 nanoparticles via C2H5OH hydrothermal reduction.JOURNAL OF ALLOYS AND COMPOUNDS,468(1-2),L5-L8.
MLA Pei, Zhenzhao,et al."Preparation of Cr2O3 nanoparticles via C2H5OH hydrothermal reduction".JOURNAL OF ALLOYS AND COMPOUNDS 468.1-2(2009):L5-L8.

入库方式: OAI收割

来源:过程工程研究所

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