Preparation of Cr2O3 nanoparticles via C2H5OH hydrothermal reduction
文献类型:期刊论文
作者 | Pei, Zhenzhao1,2; Xu, Hongbin1; Zhang, Yi1 |
刊名 | JOURNAL OF ALLOYS AND COMPOUNDS
![]() |
出版日期 | 2009-01-22 |
卷号 | 468期号:1-2页码:L5-L8 |
关键词 | Nanoparticles Hydrothermal synthesis Cr2O3 Average particle size Specific surface area |
ISSN号 | 0925-8388 |
通讯作者 | Xu, HB |
英文摘要 | Nanoparticles of chromic oxide (Cr2O3) are widely used in many fields serving as catalysts, wear resistance materials, and advanced colorants. with chromium anhydride (CrO3) and anhydrous alcohol (C2H5OH) as the raw materials, nanoparticles of Cr2O3 were successfully prepared via hydrothermal synthesis. At a reaction temperature as low as 190 C, the redox reaction could lie completed within only 1 h. The process needs no stirrer and surfactant and it was easily controllable. The obtained products were loosely agglomerated Cr2O3 nanoparticle, with an average particle size ranging from 29 nm to 60 nm. Various approaches including XRD, FE-SEM, TG-DSC, and IR were used to investigate(e the intermediate and final products. The findings show that a higher calcination temperature lends to result in a smaller specific surface area and a larger average particle size. and it higher ratio of C2H5OH to Cro(3) always leads to a higher specific surface area and therefore a smaller average particle size of (lie products. Moreover, the agglomeration of nanoparticles weakens with the increase of calcination temperature. As the process is simple and low-cost, it has the potential to lie produced oil a large scale. (c) 2008 Elsevier B.V. All rights reserved. |
WOS标题词 | Science & Technology ; Physical Sciences ; Technology |
类目[WOS] | Chemistry, Physical ; Materials Science, Multidisciplinary ; Metallurgy & Metallurgical Engineering |
研究领域[WOS] | Chemistry ; Materials Science ; Metallurgy & Metallurgical Engineering |
关键词[WOS] | CHROMIUM-OXIDE ; MAGNETIC-PROPERTIES |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000263080000002 |
公开日期 | 2013-12-11 |
版本 | 出版稿 |
源URL | [http://ir.ipe.ac.cn/handle/122111/6758] ![]() |
专题 | 过程工程研究所_湿法冶金清洁生产技术国家工程实验室 |
作者单位 | 1.Chinese Acad Sci, Inst Proc Engn, Beijing 100080, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China |
推荐引用方式 GB/T 7714 | Pei, Zhenzhao,Xu, Hongbin,Zhang, Yi. Preparation of Cr2O3 nanoparticles via C2H5OH hydrothermal reduction[J]. JOURNAL OF ALLOYS AND COMPOUNDS,2009,468(1-2):L5-L8. |
APA | Pei, Zhenzhao,Xu, Hongbin,&Zhang, Yi.(2009).Preparation of Cr2O3 nanoparticles via C2H5OH hydrothermal reduction.JOURNAL OF ALLOYS AND COMPOUNDS,468(1-2),L5-L8. |
MLA | Pei, Zhenzhao,et al."Preparation of Cr2O3 nanoparticles via C2H5OH hydrothermal reduction".JOURNAL OF ALLOYS AND COMPOUNDS 468.1-2(2009):L5-L8. |
入库方式: OAI收割
来源:过程工程研究所
浏览0
下载0
收藏0
其他版本
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。