Synthesis and Properties of Micron-size Magneic Polymer Spheres with Epoxy Groups
文献类型：期刊论文
| 作者 | Liu XQ(刘先桥) ; Guan YP(官月平) ; Xing JM(邢建民) ; Ma ZY(马志亚) ; Liu HZ(刘会洲) |
| 刊名 | Chinese Journal of Chemical Engineering
 |
| 出版日期 | 2003 |
| 期号 | 06页码:119-123 |
| 关键词 | magnetic microsphere synthesis suspension polymerization bioseparation |
| 中文摘要 | <正> Micron-size superparamagnetic poly(styrene-divinylbenzene-glycidyl methacrylate) (PSt-DVB-GMA)spheres were prepared via a modified suspension copolymerization method. Oleic acid coated magnetite (Fe_3O_4)nanoparticles made by co-precipitation were first mixed with monomers of St, DVB, GMA, and benzoyl peroxide(BPO) to form oil in water suspension with the presence of poly(vinyl pyrrolidone) (PVP-K30) as a stabilizer.Then the temperature of mixture was increased at a controlled rate to obtain small and relatively uniform droplets.Finally, the copolymerization reaction was initiated by the decomposition of BPO. The morphology and propertiesof magnetic PSt-DVB-GMA microspheres were examined by SEM, TEM, VSM, XRD and FT-IR. The magneticmicrospheres obtained have very small size (about 4-7μm) in diameter with narrow size distribution and super-paramagnetic characteristics. Powder X-ray diffraction measurements show the inverse cubic spinel structure forthe magnetite dispersed in polymer microspheres. FT-IR |
| 公开日期 | 2013-12-24 |
| 版本 | 出版稿 |
| 源URL | [http://ir.ipe.ac.cn/handle/122111/7034]  |
| 专题 | 过程工程研究所_研究所（批量导入） |
| 推荐引用方式 GB/T 7714 | Liu XQ,Guan YP,Xing JM,et al. Synthesis and Properties of Micron-size Magneic Polymer Spheres with Epoxy Groups[J]. Chinese Journal of Chemical Engineering,2003(06):119-123. |
| APA | Liu XQ,Guan YP,Xing JM,Ma ZY,&Liu HZ.(2003).Synthesis and Properties of Micron-size Magneic Polymer Spheres with Epoxy Groups.Chinese Journal of Chemical Engineering(06),119-123. |
| MLA | Liu XQ,et al."Synthesis and Properties of Micron-size Magneic Polymer Spheres with Epoxy Groups".Chinese Journal of Chemical Engineering .06(2003):119-123. |
入库方式： OAI收割
来源：过程工程研究所
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