Synthesis and characterization of zinc sulfide hollow microspheres
文献类型：期刊论文
| 作者 | Wang, J ; Song, B ; Wang, WJ ; Wu, R ; Sun, YF ; Zheng, YF ; Jian, JK |
| 刊名 | POWDER DIFFRACTION
 |
| 出版日期 | 2009 |
| 卷号 | 24期号:1页码:24 |
| 关键词 | WURTZITE-TYPE ZNS PHOTOCATALYTIC ACTIVITY SOLVOTHERMAL ROUTE OPTICAL-PROPERTIES NANOPARTICLES NANOSPHERES MORPHOLOGY NANOTUBES NANOSTRUCTURES FABRICATION |
| ISSN号 | 0885-7156 |
| 通讯作者 | Jian, JK (reprint author), Xinjiang Univ, Dept Phys, Urumqi 830046, Xinjiang, Peoples R China. |
| 中文摘要 | The successful synthesis of ZnS hollow microspheres by a solvothermal route is reported. The synthesis was achieved by a proper selection of a sulfur source, i.e., Na(2)S(2)O(3)center dot 5H(2)O or (NH(2))(2)CS, to react with Zn(CH(3)COO)(2)center dot 2H(2)O in mixed solvents of-ethylene glycol and deionized water. The ZnS products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and photoluminescence spectroscopy. XRD identified the ZnS products to have either zinc blende or wurtzite structure. SEM images revealed hollow ZnS microspheres with 1 to 2 mu m diameters and 100 to 200 nm shell thicknesses. TEM images confirmed that the hollow ZnS microspheres were assembled by ZnS crystalline nanocrystallites. The room-temperature photoluminescence spectrum of the zinc blende hollow microspheres showed a strong green emission at 514 nm and weak emission at 379 run. 0 2009 International Centre for Diffraction Data. [DOI: 10.1154/1.3079687] |
| 收录类别 | SCI |
| 资助信息 | National High Technology Research and Development Program of China [2006AA03A107]; National Natural Science Foundation of China [50702073]; National Basic Research Program of China [2007CB936300]; XiRjiang University starting fund [BS060110] |
| 语种 | 英语 |
| 公开日期 | 2013-09-24 |
| 源URL | [http://ir.iphy.ac.cn/handle/311004/54331]  |
| 专题 | 物理研究所_物理所公开发表论文_物理所公开发表论文_期刊论文 |
| 推荐引用方式 GB/T 7714 | Wang, J,Song, B,Wang, WJ,et al. Synthesis and characterization of zinc sulfide hollow microspheres[J]. POWDER DIFFRACTION,2009,24(1):24. |
| APA | Wang, J.,Song, B.,Wang, WJ.,Wu, R.,Sun, YF.,...&Jian, JK.(2009).Synthesis and characterization of zinc sulfide hollow microspheres.POWDER DIFFRACTION,24(1),24. |
| MLA | Wang, J,et al."Synthesis and characterization of zinc sulfide hollow microspheres".POWDER DIFFRACTION 24.1(2009):24. |
入库方式： OAI收割
来源：物理研究所
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