Pyrolysis synthesis and microstructure of zirconium carbide from new preceramic polymers
文献类型：期刊论文
| 作者 | Wu, Haitang1; Zhang, Weigang2; Zhang, Junhua1 |
| 刊名 | CERAMICS INTERNATIONAL
 |
| 出版日期 | 2014-05-01 |
| 卷号 | 40期号:4页码:5967-5972 |
| 关键词 | Pyrolysis Precursor Zirconium carbide Ceramics Microstructure |
| ISSN号 | 0272-8842 |
| 其他题名 | Ceram. Int. |
| 中文摘要 | ZrC was synthesized by pyrolysis of a novel polymeric precursor, which was prepared from the reaction of zirconium tetrachloride with acetylacetone, methanol and 1,4-butanediol. The pyrolysis behavior and structural evolution of the precursor, the microstructure and composition of the synthesized ZrC particle were fully investigated. The results showed that the precursor could completely transform into ZrC after heat treatment in argon at temperatures above 1400 degrees C. However, the initial formation temperature of ZrC was as low as 1200 degrees C whereas ZrO2 as an intermediate product was also produced from the precursor at 1000 degrees C, and the mixture was finally transformed into pure ZrC at elevated temperatures. The obtained ZrC particles exhibited face-centered cubic lattice structures with the size ranging from 50 to 100 nm. (c) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved. |
| 英文摘要 | ZrC was synthesized by pyrolysis of a novel polymeric precursor, which was prepared from the reaction of zirconium tetrachloride with acetylacetone, methanol and 1,4-butanediol. The pyrolysis behavior and structural evolution of the precursor, the microstructure and composition of the synthesized ZrC particle were fully investigated. The results showed that the precursor could completely transform into ZrC after heat treatment in argon at temperatures above 1400 degrees C. However, the initial formation temperature of ZrC was as low as 1200 degrees C whereas ZrO2 as an intermediate product was also produced from the precursor at 1000 degrees C, and the mixture was finally transformed into pure ZrC at elevated temperatures. The obtained ZrC particles exhibited face-centered cubic lattice structures with the size ranging from 50 to 100 nm. (c) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved. |
| WOS标题词 | Science & Technology ; Technology |
| 类目[WOS] | Materials Science, Ceramics |
| 研究领域[WOS] | Materials Science |
| 关键词[WOS] | HIGH-TEMPERATURE SYNTHESIS ; ZRC ; COMPOSITES ; FABRICATION ; POWDERS ; PRECURSORS ; CERAMICS ; EVOLUTION ; MATRIX ; CARBON |
| 收录类别 | SCI |
| 原文出处 | |
| 语种 | 英语 |
| WOS记录号 | WOS:000332268200113 |
| 公开日期 | 2014-05-06 |
| 版本 | 出版稿 |
| 源URL | [http://ir.ipe.ac.cn/handle/122111/8181]  |
| 专题 | 过程工程研究所_研究所（批量导入） |
| 作者单位 | 1.Northwest A&F Univ, Coll Forestry, Yangling 712100, Peoples R China 2.Chinese Acad Sci, Inst Proc Engn, State Key Lab Multi Phase Complex Syst, Beijing 100190, Peoples R China |
| 推荐引用方式 GB/T 7714 | Wu, Haitang,Zhang, Weigang,Zhang, Junhua. Pyrolysis synthesis and microstructure of zirconium carbide from new preceramic polymers[J]. CERAMICS INTERNATIONAL,2014,40(4):5967-5972. |
| APA | Wu, Haitang,Zhang, Weigang,&Zhang, Junhua.(2014).Pyrolysis synthesis and microstructure of zirconium carbide from new preceramic polymers.CERAMICS INTERNATIONAL,40(4),5967-5972. |
| MLA | Wu, Haitang,et al."Pyrolysis synthesis and microstructure of zirconium carbide from new preceramic polymers".CERAMICS INTERNATIONAL 40.4(2014):5967-5972. |
入库方式： OAI收割
来源：过程工程研究所
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