Using Lanthanum Fluoride Fine Particles as Stationary Phase for Thin-Layer Chromatography/Fourier Transform Infrared Spectroscopy Analysis
文献类型：期刊论文
| 作者 | Zhu, Qing1,2; Wu, Haijun1,3; Wang, Fang1,4; He, Anqi1; Huang, Kun5; Wei, Yongju4; Liu, Cuige4; Zhai, Yanjun2; Weng, Shifu1; Yang, Zhanlan1 |
| 刊名 | JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC
 |
| 出版日期 | 2014-04-01 |
| 卷号 | 27期号:2页码:80-83 |
| 关键词 | Thin-layer chromatography Fourier transform infrared spectroscopy Lanthanum fluoride Nano In situ |
| ISSN号 | 0933-4173 |
| 其他题名 | JPC-J. Planar Chromatogr.-Mod. TLC |
| 中文摘要 | While in situ TLC/FTIR technique has tremendous potential in the analysis of complex mixtures, the conventional stationary phase, such as silica gel, used for TLC/FTIR analysis, has strong absorption in IR region and thus brings about severe interference in the obtained FTIR spectra of the separated samples. In this work, we propose to use lanthanum fluoride fine particles as a new stationary phase of a TLC plate. The average size of LaF3 particles is around 100 nm. FTIR spectrum of the LaF3 particles has no interfering absorption. Preliminary TLC experiments show that mixtures of rhodamine B and methylene blue mixture can be successfully separated by this new TLC plate using LaF3 fine particles as a stationary phase. Methylene blue and rhodamine B from separated spot can be clearly detected by using in situ FTIR spectra. |
| 英文摘要 | While in situ TLC/FTIR technique has tremendous potential in the analysis of complex mixtures, the conventional stationary phase, such as silica gel, used for TLC/FTIR analysis, has strong absorption in IR region and thus brings about severe interference in the obtained FTIR spectra of the separated samples. In this work, we propose to use lanthanum fluoride fine particles as a new stationary phase of a TLC plate. The average size of LaF3 particles is around 100 nm. FTIR spectrum of the LaF3 particles has no interfering absorption. Preliminary TLC experiments show that mixtures of rhodamine B and methylene blue mixture can be successfully separated by this new TLC plate using LaF3 fine particles as a stationary phase. Methylene blue and rhodamine B from separated spot can be clearly detected by using in situ FTIR spectra. |
| WOS标题词 | Science & Technology ; Physical Sciences |
| 类目[WOS] | Chemistry, Analytical |
| 研究领域[WOS] | Chemistry |
| 关键词[WOS] | PLANAR CHROMATOGRAPHY ; PHOTOACOUSTIC-SPECTROSCOPY ; SPECTROMETRY ; RAMAN ; SPOTS |
| 收录类别 | SCI |
| 原文出处 | |
| 语种 | 英语 |
| WOS记录号 | WOS:000332956500002 |
| 公开日期 | 2014-05-06 |
| 版本 | 出版稿 |
| 源URL | [http://ir.ipe.ac.cn/handle/122111/8233]  |
| 专题 | 过程工程研究所_研究所（批量导入） |
| 作者单位 | 1.Peking Univ, Coll Chem & Mol Engn, Beijing 100871, Peoples R China 2.Liaoning Univ Tradit Chinese Med, Coll Pharm, Dalian 116600, Peoples R China 3.Inner Mongolia Univ Nationalities, Mongolia Med Coll, Tongliao 028000, Peoples R China 4.Hebei Normal Univ, Coll Chem & Mat Sci, Shijiazhuang 050024, Peoples R China 5.Chinese Acad Sci, Inst Proc Engn, Beijing 100190, Peoples R China 6.Univ Delaware, Dept Mat Sci & Engn, Newark, DC 19716 USA |
| 推荐引用方式 GB/T 7714 | Zhu, Qing,Wu, Haijun,Wang, Fang,et al. Using Lanthanum Fluoride Fine Particles as Stationary Phase for Thin-Layer Chromatography/Fourier Transform Infrared Spectroscopy Analysis[J]. JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC,2014,27(2):80-83. |
| APA | Zhu, Qing.,Wu, Haijun.,Wang, Fang.,He, Anqi.,Huang, Kun.,...&Wu, Jinguang.(2014).Using Lanthanum Fluoride Fine Particles as Stationary Phase for Thin-Layer Chromatography/Fourier Transform Infrared Spectroscopy Analysis.JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC,27(2),80-83. |
| MLA | Zhu, Qing,et al."Using Lanthanum Fluoride Fine Particles as Stationary Phase for Thin-Layer Chromatography/Fourier Transform Infrared Spectroscopy Analysis".JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC 27.2(2014):80-83. |
入库方式： OAI收割
来源：过程工程研究所
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