Selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in soil matrices
文献类型：期刊论文
| 作者 | Teng Man ; Jin Jing ; Fu Qiang ; Cai YaQi ; Chen JiPing ; Wei FuSheng |
| 刊名 | CHINESE SCIENCE BULLETIN
 |
| 出版日期 | 2013 |
| 卷号 | 58期号:41734页码:500-506 |
| 通讯作者 | Cai, YQ |
| 中文摘要 | A method for the selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in complex matrices was developed. In the present study, the type of sorbents and the volume and composition of eluting solvents were investigated in detail. Under the optimal conditions, the recoveries of PCNs, HBCDs and TBBPA in different fractions were determined with liquid/gas chromatography tandem mass spectrometry (LC or GC-MS/MS), which was nearly close to 100%. To investigate the feasibility of the developed method, it was applied to isolate target compounds from spiked soil extracts. PCNs, HBCDs and TBBPA could be subsequently eluted with hexane, hexane/dichloromethane (1: 1), and hexane/dichloromethane (1: 3), and the recoveries of the analysts from three fractions were satisfactory (70.9%-107%) with the exception of gamma-HBCD at low levels. The results indicated that the method exhibited good performance for the selective separation of PCNs, HBCDs and TBBPA and showed great potential in sample pretreatment in terms of alleviating influence from different class of impurities to some extent. |
| 收录类别 | SCI |
| WOS记录号 | WOS:000315445500010 |
| 公开日期 | 2014-06-06 |
| 源URL | [http://ir.rcees.ac.cn/handle/311016/7532]  |
| 专题 | 生态环境研究中心_环境化学与生态毒理学国家重点实验室 |
| 推荐引用方式 GB/T 7714 | Teng Man,Jin Jing,Fu Qiang,et al. Selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in soil matrices[J]. CHINESE SCIENCE BULLETIN,2013,58(41734):500-506. |
| APA | Teng Man,Jin Jing,Fu Qiang,Cai YaQi,Chen JiPing,&Wei FuSheng.(2013).Selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in soil matrices.CHINESE SCIENCE BULLETIN,58(41734),500-506. |
| MLA | Teng Man,et al."Selective separation of polychlorinated naphthalene (PCNs), hexabromocyclododecanes (HBCDs) and tetrabromobisphenol A (TBBPA) in soil matrices".CHINESE SCIENCE BULLETIN 58.41734(2013):500-506. |
入库方式： OAI收割
来源：生态环境研究中心
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。