Heat capacities and thermodynamic properties of Ni-9(btz)(12)(DMA)(6)(NO3)(6)
文献类型：期刊论文
| 作者 | Zhou, Yi-Xi1,2; Sun, Li-Xian1; Cao, Zhong2; Xu, Fen3; Jiang, Chun-Hong1; Jiao, Cheng-Li1; Zhang, Hui1,2; Zhang, Jian1; Zhou, Huai-Ying4; Li, Fen1 |
| 刊名 | journal of thermal analysis and calorimetry
 |
| 出版日期 | 2013-02-01 |
| 卷号 | 111期号:2页码:1603-1608 |
| 关键词 | Crystalline Molar heat capacity TG TMDSC |
| 产权排序 | 待补充 |
| 通讯作者 | 孙立贤 |
| 合作状况 | 英 |
| 英文摘要 | the low-temperature molar heat capacity of crystalline ni-9(btz)(12)(dma)(6)(no3)(6) (1) (btz = benzotriazolate; dma = n,n'-dimethylacetamide) was measured by temperature-modulated differential scanning calorimetry for the first time. the thermodynamic parameters such as entropy and enthalpy relative to reference temperature 298.15 k were obtained based on the above molar heat capacity data. the compound was synthesized by solvothermal method and characterized by powder x-ray diffraction and ft-ir spectra. moreover, the thermal stability and the decomposition mechanism of ni-9(btz)(12)(dma)(6)(no3)(6) were investigated by thermogravimetry (tg) analysis under air atmosphere from 300 to 873 k. the experimental results through tg measurement demonstrate that the compound has a two-stage mass loss in air flow. |
| WOS标题词 | science & technology ; physical sciences |
| 学科主题 | 物理化学 |
| 类目[WOS] | chemistry, analytical ; chemistry, physical |
| 研究领域[WOS] | chemistry |
| 关键词[WOS] | storage materials ; dsc ; nanostructures ; temperature ; polymer |
| 收录类别 | SCI |
| 资助信息 | 1，1 |
| 原文出处 | 1608 |
| 语种 | 英语 |
| WOS记录号 | WOS:000313409700077 |
| 公开日期 | 2014-09-11 |
| 源URL | [http://159.226.238.44/handle/321008/119236]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Mat & Thermochem Lab, Dalian 116023, Peoples R China 2.Changsha Univ Sci & Technol, Sch Chem & Biol Engn, Changsha 410004, Hunan, Peoples R China 3.Liaoning Normal Univ, Fac Chem & Chem Engn, Dalian 116029, Peoples R China 4.Guilin Univ Elect Technol, Dept Mat Sci & Engn, Guilin 541004, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhou, Yi-Xi,Sun, Li-Xian,Cao, Zhong,et al. Heat capacities and thermodynamic properties of Ni-9(btz)(12)(DMA)(6)(NO3)(6)[J]. journal of thermal analysis and calorimetry,2013,111(2):1603-1608. |
| APA | Zhou, Yi-Xi.,Sun, Li-Xian.,Cao, Zhong.,Xu, Fen.,Jiang, Chun-Hong.,...&Zhang, Huang-Zhi.(2013).Heat capacities and thermodynamic properties of Ni-9(btz)(12)(DMA)(6)(NO3)(6).journal of thermal analysis and calorimetry,111(2),1603-1608. |
| MLA | Zhou, Yi-Xi,et al."Heat capacities and thermodynamic properties of Ni-9(btz)(12)(DMA)(6)(NO3)(6)".journal of thermal analysis and calorimetry 111.2(2013):1603-1608. |
入库方式： OAI收割
来源：大连化学物理研究所
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