Synthesis of molecularly imprinted polymer sorbents and application for the determination of aminoglycosides antibiotics in honey
文献类型：期刊论文
| 作者 | Ji, Shunli1; Zhang, Feifang1; Luo, Xi1; Yang, Bingcheng1; Jin, Gaowa2; Yan, Jingyu2; Liang, Xinmiao1,2 |
| 刊名 | journal of chromatography a
 |
| 出版日期 | 2013-10-25 |
| 卷号 | 1313页码:113-118 |
| 关键词 | Molecularly imprinted polymer HILIC-MS/MS Aminoglycoside antibiotics Solid phase extraction Honey samples |
| 产权排序 | 待补充 |
| 通讯作者 | 杨丙成 |
| 合作状况 | 英 |
| 英文摘要 | aminoglycoside antibiotic (aa)-selective molecularly imprinted polymer (mip) sorbent was synthesized by polymerization of methacrylic acid and ethylene glycol dimethacrylate in the presence of streptomycin as template molecule. the mip sorbent was in detail characterized and its performance was evaluated by selecting four model aas including streptomycin, gentamicin, spectinomycin and dihydrostreptomycin. relative to non-imprinted polymer (nip), the mips exhibited much higher recognizable capacity and specificity to the aas and negligible adsorption for non-aas as well. in combination of hydrophilic interaction liquid chromatography-tandem mass spectrometry (hilic-ms/ms), the mip sorbent-based solid phase extraction (spe) was able to effectively determine the residue of four model aas in honey samples with recovery ranging from 90% to 110%. the limit of detection (and the limit of quantitation) of streptomycin, gentamicin, spectinomycin and dihydrostreptomycin was 4.5 (15.0), 2.4 (8.0), 6.0 (20.0) and 1.8 (6.0) mu g/kg, respectively. relative standard deviations of intraday and inter-day assay under three spiked levels were 4.4-12.0% and 6.8-14.6%, respectively. (c) 2013 elsevier b.v. all rights reserved. |
| WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
| 学科主题 | 物理化学 |
| 类目[WOS] | biochemical research methods ; chemistry, analytical |
| 研究领域[WOS] | biochemistry & molecular biology ; chemistry |
| 关键词[WOS] | solid-phase microextraction ; chromatography/tandem mass-spectrometry ; liquid-chromatography ; hydrophilic interaction ; extraction ; samples ; fluoroquinolones ; streptomycin ; recognition ; separation |
| 收录类别 | SCI |
| 资助信息 | 2，5 |
| 原文出处 | 118 |
| 语种 | 英语 |
| WOS记录号 | WOS:000325673200010 |
| 公开日期 | 2014-09-11 |
| 源URL | [http://159.226.238.44/handle/321008/119343]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China 2.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China |
| 推荐引用方式 GB/T 7714 | Ji, Shunli,Zhang, Feifang,Luo, Xi,et al. Synthesis of molecularly imprinted polymer sorbents and application for the determination of aminoglycosides antibiotics in honey[J]. journal of chromatography a,2013,1313:113-118. |
| APA | Ji, Shunli.,Zhang, Feifang.,Luo, Xi.,Yang, Bingcheng.,Jin, Gaowa.,...&Liang, Xinmiao.(2013).Synthesis of molecularly imprinted polymer sorbents and application for the determination of aminoglycosides antibiotics in honey.journal of chromatography a,1313,113-118. |
| MLA | Ji, Shunli,et al."Synthesis of molecularly imprinted polymer sorbents and application for the determination of aminoglycosides antibiotics in honey".journal of chromatography a 1313(2013):113-118. |
入库方式： OAI收割
来源：大连化学物理研究所
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