Simultaneous determination of mono- and disubstituted polyfluoroalkyl phosphates in drinking water by liquid chromatography-electrospray tandem mass spectrometry
文献类型：期刊论文
| 作者 | Ding, Huanhuan ; Peng, Hui ; Yang, Min ; Hu, Jianying |
| 刊名 | JOURNAL OF CHROMATOGRAPHY A
 |
| 出版日期 | 2012 |
| 卷号 | 1227页码:245－252 |
| 关键词 | Disubstituted polyfluoroalkyl phosphates Monosubstituted polyfluoroalkyl phosphates WAX cartridge LC-MS/MS Drinking water |
| ISSN号 | 0021-9673 |
| 中文摘要 | A sensitive liquid chromatography-electrospray tandem mass spectrometry method was established for the simultaneous determination of five monosubstituted polyfluoroalkyl phosphates (monoPAPs) and eight disubstituted polyfluoroalkyl phosphates (diPAPs) in drinking water. Complete separation and good retention for 13 polyfluoroalkyls phosphates (PAPs) were achieved with a Waters ACUITY UPLC BEH C8 column using a mixture of methanol/water containing 0.1% NH4OH as the mobile phases. Extraction of drinking water samples was performed on weak anion exchange (WAX) cartridges, and the recoveries of target compounds were from 65 to 110%. The limits of quantization (LOQs) for 13 analytes were in the range of 0.4-40 ng/L. This method was applied to analyze the PAPs in drinking water samples from three cities in China. Of the 13 PAPs, six PAPs including 6:2 monoPAP (13.0 ng/L), 8:2 monoPAP (3.6 ng/L), 10:1 monoPAP (4.3-70.3 ng/L), 10:2 monoPAP (1.4-5.6 ng/L), 8:2 diPAP (0.10 ng/L), and 10:1 diPAP (0.8-3.8 ng/L) were detected. (C) 2012 Elsevier B.V. All rights reserved. |
| WOS记录号 | WOS:000301563700027 |
| 公开日期 | 2014-11-04 |
| 源URL | [http://ir.rcees.ac.cn/handle/311016/7833]  |
| 专题 | 生态环境研究中心_环境水质学国家重点实验室 |
| 推荐引用方式 GB/T 7714 | Ding, Huanhuan,Peng, Hui,Yang, Min,et al. Simultaneous determination of mono- and disubstituted polyfluoroalkyl phosphates in drinking water by liquid chromatography-electrospray tandem mass spectrometry[J]. JOURNAL OF CHROMATOGRAPHY A,2012,1227:245－252. |
| APA | Ding, Huanhuan,Peng, Hui,Yang, Min,&Hu, Jianying.(2012).Simultaneous determination of mono- and disubstituted polyfluoroalkyl phosphates in drinking water by liquid chromatography-electrospray tandem mass spectrometry.JOURNAL OF CHROMATOGRAPHY A,1227,245－252. |
| MLA | Ding, Huanhuan,et al."Simultaneous determination of mono- and disubstituted polyfluoroalkyl phosphates in drinking water by liquid chromatography-electrospray tandem mass spectrometry".JOURNAL OF CHROMATOGRAPHY A 1227(2012):245－252. |
入库方式： OAI收割
来源：生态环境研究中心
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