Preparation of Pseudo-boehmite and gamma-Al2O3 by Polyaluminum Chloride II -Surfactant Influences
文献类型:期刊论文
作者 | Wang Yuan-Yuan ; Zhao Chang-Wei ; He Jin-Song ; Yan Yong ; Zhang Xiang-Lan ; Luan Zhao-Kun |
刊名 | Chemistry
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出版日期 | 2012 |
卷号 | 28期号:2页码:302-306 |
关键词 | polyaluminum chloride pseudo-hoe-halite gamma-Al2O3 pluronic |
ISSN号 | 1001-4861 |
中文摘要 | Pseudo-boehmite and its derivative gamma-Al2O3 were prepared from polyaluminum chloride by sol-gel method. The samples were characterized by XRD, TEM and N-2, adsorption-desorption techniques. Effects of pH value, preparation temperature and species of pluronic surfactants on the physical properties of pseudo-boehmite were investigated. Results show that alumina hydrate is mainly pseudo-boehmite prepared at pH value near 8.5 and at temperature value near 70 degrees C. With the increase of pluronic surfactants molecular weight, the degree of crystallinity of pseudo-boehmite and its derivative gamma-Al2O3 increases. It is proved that phases of products do not change after adding the pluronic surfactants L64, L65 and F68. The gamma-Al2O3 phases are obtained after 6 hours calcination of the pseudo-boehmite at 500 degrees C. L65 is the most suitable for increasing surface area of gamma-Al2O3, surface area of 231 m(2).g(-1), pore volume of 0.28 cm(3).g(-1) and pore size of 4.52 nm was obtained. |
WOS记录号 | WOS:000300746000016 |
公开日期 | 2014-11-28 |
源URL | [http://ir.rcees.ac.cn/handle/311016/8160] ![]() |
专题 | 生态环境研究中心_环境水质学国家重点实验室 |
推荐引用方式 GB/T 7714 | Wang Yuan-Yuan,Zhao Chang-Wei,He Jin-Song,et al. Preparation of Pseudo-boehmite and gamma-Al2O3 by Polyaluminum Chloride II -Surfactant Influences[J]. Chemistry,2012,28(2):302-306. |
APA | Wang Yuan-Yuan,Zhao Chang-Wei,He Jin-Song,Yan Yong,Zhang Xiang-Lan,&Luan Zhao-Kun.(2012).Preparation of Pseudo-boehmite and gamma-Al2O3 by Polyaluminum Chloride II -Surfactant Influences.Chemistry,28(2),302-306. |
MLA | Wang Yuan-Yuan,et al."Preparation of Pseudo-boehmite and gamma-Al2O3 by Polyaluminum Chloride II -Surfactant Influences".Chemistry 28.2(2012):302-306. |
入库方式: OAI收割
来源:生态环境研究中心
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