The synthesis of flower shaped microstructures of Co3O4 by solvothermal approach and investigation of its catalytic activity
文献类型：期刊论文
| 作者 | Jamil, Saba; Janjua, Muhammad Ramzan Saeed Ashraf; Ahmad, Tauqeer |
| 刊名 | Solid State Sciences
 |
| 出版日期 | 2014 |
| 卷号 | 36期号:10页码:73-79 |
| 关键词 | Nanosheets Chemical synthesis Differential scanning calorimetry (DSC) Thermo gravimetric analysis (TGA) Catalytic properties |
| ISSN号 | 12932558 |
| 英文摘要 | A unique flower like microstructures of cobalt oxide (Co3O 4) are prepared by solvothermal method in two steps: In first step the Co(OH)2 micro particles are generated and in second step Co 3O4 flower like microstructures are obtained after annealing for 2 h. The final product of Co3O4 is subjected to different instrumental analysis to investigate its morphology and other properties. It is clear from the Scanning Electron Microscopy (SEM) and Transmission Electron Microscopy (TEM) that the product is flower like in shape with a size of approximately 10-15 μm from sideway view. It is also observed that these structures are composed of nanosheets, which are further organized into layer by layer pattern to form a specific flower like morphology. The experimental data proved that the solvent and temperature played a significant role in the formation of such flowers like morphology under provided reaction conditions. These microstructures have shown remarkable catalytic activity for thermal decomposition of ammonium perchlorate (AP). |
| 收录类别 | SCI |
| WOS记录号 | WOS:000343382100011 |
| 公开日期 | 2014-11-11 |
| 源URL | [http://ir.xjipc.cas.cn/handle/365002/4023]  |
| 专题 | 新疆理化技术研究所_中国科学院特殊环境功能材料与器件重点试验室 |
| 作者单位 | Univ Sargodha, Dept Chem, Sargodha 40100, Pakistan;Harbin Engn Univ, Key Lab Superlight Mat & Surface Technol, Minist Educ, Harbin 150001, Peoples R China;Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Xinjiang Key Lab Elect Informat Mat & Devices, Key Lab Funct Mat & Devices Special Environm, Urumqi 830011, Peoples R China |
| 推荐引用方式 GB/T 7714 | Jamil, Saba,Janjua, Muhammad Ramzan Saeed Ashraf,Ahmad, Tauqeer. The synthesis of flower shaped microstructures of Co3O4 by solvothermal approach and investigation of its catalytic activity[J]. Solid State Sciences,2014,36(10):73-79. |
| APA | Jamil, Saba,Janjua, Muhammad Ramzan Saeed Ashraf,&Ahmad, Tauqeer.(2014).The synthesis of flower shaped microstructures of Co3O4 by solvothermal approach and investigation of its catalytic activity.Solid State Sciences,36(10),73-79. |
| MLA | Jamil, Saba,et al."The synthesis of flower shaped microstructures of Co3O4 by solvothermal approach and investigation of its catalytic activity".Solid State Sciences 36.10(2014):73-79. |
入库方式： OAI收割
来源：新疆理化技术研究所
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