A polar-embedded C30 stationary phase: Preparation and evaluation
文献类型：期刊论文
| 作者 | Zhang ML(张明亮)1,2,3; Mai WP(买文鹏)4; Zhao L(赵亮)1,2 ; Guo Y(郭勇)1,2; Qiu HD(邱洪灯)1,2; Qiu HD(邱洪灯)
|
| 刊名 | Journal of Chromatography A
 |
| 出版日期 | 2015 |
| 卷号 | 1388页码:133-140 |
| 关键词 | Polar-embedded Carbamate Triacontyl chain Shape selectivity Reversed-phase liquid chromatography |
| ISSN号 | 0021-9673 |
| 通讯作者 | 邱洪灯 |
| 英文摘要 | A novel polar-embedded C30 stationary phase has been synthesized and characterized. The polar car-bamate group was generated homogeneously in situ by the catalytic reaction between isocyanate andprimary alcohol. The simple one-pot synthetic strategy provided an efficient and effective strategy formodification of silica spheres. Efficiency, selectivity and silanol activity of the resulting column were char-acterized in detail with different classes of analytes that included Standard Reference Materials (SRM)870, SRM 869b and SRM 1647e, alkylbenzene congeners, as well as polar-substituted aromatics. Thepolar-embedded C30 stationary phase was found to exhibit excellent shape selectivity. |
| 学科主题 | 分析化学与药物化学 |
| 收录类别 | SCI |
| 资助信息 | the “Hun-dred Talents Program” of Chinese Academy of Sciences;the National Natural Science Foundation of China (Nos. 21405163;21475142) |
| 语种 | 英语 |
| WOS记录号 | WOS:000351792400016 |
| 公开日期 | 2015-03-11 |
| 源URL | [http://210.77.64.217/handle/362003/7158]  |
| 专题 | 兰州化学物理研究所_中科院西北特色植物资源化学重点实验室/甘肃省天然药物重点实验室 |
| 通讯作者 | Qiu HD(邱洪灯) |
| 作者单位 | 1.Chinese Acad Sci, Key Lab Chem Northwestern Plant Resources, Lanzhou 730000, Peoples R China 2.Chinese Acad Sci, Key Lab Nat Med Gansu Prov, Lanzhou Inst Chem Phys, Lanzhou 730000, Peoples R China 3.Chinese Acad Sci, Univ Chinese Acad Sci, Beijing 100049, Peoples R China 4.Henan Univ Technol, Sch Chem & Chem Engn, Zhengzhou 450001, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhang ML,Mai WP,Zhao L,et al. A polar-embedded C30 stationary phase: Preparation and evaluation[J]. Journal of Chromatography A,2015,1388:133-140. |
| APA | Zhang ML,Mai WP,Zhao L,Guo Y,Qiu HD,&邱洪灯.(2015).A polar-embedded C30 stationary phase: Preparation and evaluation.Journal of Chromatography A,1388,133-140. |
| MLA | Zhang ML,et al."A polar-embedded C30 stationary phase: Preparation and evaluation".Journal of Chromatography A 1388(2015):133-140. |
入库方式： OAI收割
来源：兰州化学物理研究所
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