Determination of Bromothalonil Residues and Degradation in Apple and Soil by QuEChERS and GC-MS/MS
文献类型:期刊论文
作者 | Wang, Huili![]() |
刊名 | BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY
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出版日期 | 2014 |
卷号 | 92期号:4页码:451-454 |
关键词 | QuEChERS Bromothalonil Apple Soil Residue Dissipation |
ISSN号 | 0007-4861 |
中文摘要 | The dissipation and residues of bromothalonil in apple and soil under field condition were analyzed by QuEChERS (quick, easy, cheap, effective, rugged and safe) combined with gas chromatography-mass spectrometer method. The recoveries were ranged from 80.8 % to 106 % with coefficient variation for repeatability ranged from 3.08 % to 7.09 % at fortification levels of 0.02, 0.04 and 0.2 mg/kg in apple and soil. The limit of quantification of the method was 0.31 mu g/kg. The dissipation rates of bromothalonil followed the first-order kinetics and the half-lives were from 3.61 to 3.98 days in apple and from 4.65 to 9.29 days in soil. In apple, the terminal residues of bromothalonil were below the China maximum residue limit (0.2 mg/kg) after 7 days of application. This work contributed to provide the basic information for a safe usage of bromothalonil in apple orchard and preventing health problem from consumers in China. |
WOS记录号 | WOS:000332797900014 |
公开日期 | 2015-03-26 |
源URL | [http://ir.rcees.ac.cn/handle/311016/9653] ![]() |
专题 | 生态环境研究中心_中国科学院环境生物技术重点实验室 |
推荐引用方式 GB/T 7714 | Wang, Huili. Determination of Bromothalonil Residues and Degradation in Apple and Soil by QuEChERS and GC-MS/MS[J]. BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY,2014,92(4):451-454. |
APA | Wang, Huili.(2014).Determination of Bromothalonil Residues and Degradation in Apple and Soil by QuEChERS and GC-MS/MS.BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY,92(4),451-454. |
MLA | Wang, Huili."Determination of Bromothalonil Residues and Degradation in Apple and Soil by QuEChERS and GC-MS/MS".BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY 92.4(2014):451-454. |
入库方式: OAI收割
来源:生态环境研究中心
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