Synthesis and electrical conductivity of nanocrystalline tetragonal FeS
文献类型：期刊论文
| 作者 | Zeng, SL ; Wang, HX ; Dong, C |
| 刊名 | CHINESE PHYSICS B
 |
| 出版日期 | 2014 |
| 卷号 | 23期号:8 |
| 关键词 | tetragonal FeS synthesis method electrical conductivity grain boundary |
| ISSN号 | 1674-1056 |
| 通讯作者 | Dong, C (reprint author), Chinese Acad Sci, Beijing Natl Lab Condensed Matter Phys, Inst Phys, Beijing 100190, Peoples R China. |
| 中文摘要 | A convenient method for synthesis of tetragonal FeS using iron powder as iron source, is reported. Nanocrystalline tetragonal FeS samples were successfully synthesized by reacting metallic iron powder with sodium sulfide in acetate buffer solution. The obtained sample is single-phase tetragonal FeS with lattice parameters a - 0.3767 nm and c - 0.5037 nm, as revealed by X-ray diffraction. The sample consists of flat nanosheets with lateral dimensions from 20 nm up to 200 nm and average thickness of about 20 nm. We found that tetragonal FeS is a fairly good conductor from the electrical resistivity measurement on a pellet of the nanosheets. The temperature dependence of conductivity of the pellet was well fitted using an empirical equation wherein the effect of different grain boundaries was taken into consideration. This study provides a convenient, economic way to synthesize tetragonal FeS in a large scale and reports the first electrical conductivity data for tetragonal FeS down to liquid helium temperature. |
| 资助信息 | National Natural Science Foundation of China [21271183]; National Basic Research Program of China [2011CBA00112, 2011CB808202] |
| 语种 | 英语 |
| 公开日期 | 2015-04-14 |
| 源URL | [http://ir.iphy.ac.cn/handle/311004/58990]  |
| 专题 | 物理研究所_物理所公开发表论文_物理所公开发表论文_期刊论文 |
| 推荐引用方式 GB/T 7714 | Zeng, SL,Wang, HX,Dong, C. Synthesis and electrical conductivity of nanocrystalline tetragonal FeS[J]. CHINESE PHYSICS B,2014,23(8). |
| APA | Zeng, SL,Wang, HX,&Dong, C.(2014).Synthesis and electrical conductivity of nanocrystalline tetragonal FeS.CHINESE PHYSICS B,23(8). |
| MLA | Zeng, SL,et al."Synthesis and electrical conductivity of nanocrystalline tetragonal FeS".CHINESE PHYSICS B 23.8(2014). |
入库方式： OAI收割
来源：物理研究所
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。