中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Development of narrow-band TLC plates for TLC/FTIR analysis

文献类型:期刊论文

作者Wang, Fang1,2; Wu, Haijun2,3; Zhu, Qing2,4; Huang, Kun5; Wei, Yongju1; Liu, Cuige1; Zhai, Yanjun3; Yang, Zhanlan2; Weng, Shifu2; Xu, Yizhuang2
刊名ANALYTICAL METHODS
出版日期2013
卷号5期号:16页码:4138-4144
英文摘要The present paper focuses on the development of narrow-band thin-layer chromatography (TLC) coupled with Fourier transform Infrared spectroscopy (FTIR) technique. We adopted a new method to prepare a narrow-band TLC plate by using silver iodide as stationary phase. The narrow-band TLC plate exhibits a variety of advantages: the preparation time is about 20 minutes, while 3-7 days are needed to prepare a common TLC plate suitable for TLC/FTIR analysis by using "settlement volatilization method". Furthermore, the usage of stationary phase in narrow-band TLC plates decreases by about one order of magnitude in comparison with that of common TLC plates. This is very important for an expensive stationary phase such as silver iodide. In addition, experimental results of TLC/FTIR analysis on mixed samples containing rhodamine B and bromocresol green demonstrate the detection limit significantly improves by using the narrow-band TLC technique.
WOS标题词Science & Technology ; Physical Sciences ; Life Sciences & Biomedicine ; Technology
类目[WOS]Chemistry, Analytical ; Food Science & Technology ; Spectroscopy
研究领域[WOS]Chemistry ; Food Science & Technology ; Spectroscopy
关键词[WOS]THIN-LAYER-CHROMATOGRAPHY ; INFRARED PHOTOACOUSTIC-SPECTROSCOPY ; FOURIER-TRANSFORM SPECTROMETRY ; PLANAR CHROMATOGRAPHY ; STATIONARY-PHASE ; FINE PARTICLES ; MICROSCOPY ; SEPARATION
收录类别SCI
语种英语
WOS记录号WOS:000323226800053
公开日期2015-05-27
源URL[http://ir.ipe.ac.cn/handle/122111/13616]  
专题过程工程研究所_研究所(批量导入)
作者单位1.Hebei Normal Univ, Coll Chem & Mat Sci, Shijiazhuang 050024, Peoples R China
2.Peking Univ, Coll Chem & Mol Engn, Beijing 100871, Peoples R China
3.Inner Mongolia Univ Nationalities, Mongolia Med Coll, Tongliao 028000, Peoples R China
4.Liaoning Univ Tradit Chinese Med, Coll Pharm, Dalian 116600, Peoples R China
5.Chinese Acad Sci, Inst Proc Engn, Beijing 100190, Peoples R China
6.Univ Delaware, Dept Mat Sci & Engn, Newark, DE 19716 USA
推荐引用方式
GB/T 7714
Wang, Fang,Wu, Haijun,Zhu, Qing,et al. Development of narrow-band TLC plates for TLC/FTIR analysis[J]. ANALYTICAL METHODS,2013,5(16):4138-4144.
APA Wang, Fang.,Wu, Haijun.,Zhu, Qing.,Huang, Kun.,Wei, Yongju.,...&Wu, Jinguang.(2013).Development of narrow-band TLC plates for TLC/FTIR analysis.ANALYTICAL METHODS,5(16),4138-4144.
MLA Wang, Fang,et al."Development of narrow-band TLC plates for TLC/FTIR analysis".ANALYTICAL METHODS 5.16(2013):4138-4144.

入库方式: OAI收割

来源:过程工程研究所

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