Recycling and Reuse of Ionic Liquid in Homogeneous Cellulose Acetylation
文献类型：期刊论文
| 作者 | Huang Kelin1,2; Wu Rui2; Cao Yan3; Li Huiquan3; Wang Jinshu1 |
| 刊名 | CHINESE JOURNAL OF CHEMICAL ENGINEERING
 |
| 出版日期 | 2013-05-01 |
| 卷号 | 21期号:5页码:577-584 |
| 关键词 | cellulose ionic liquid molecular distillation recycling |
| 英文摘要 | Molecular distillation was used to recover ionic liquid (IL) 1-ally1-3-methylimidazolium chloride (AmimC1) in homogeneous cellulose acetylation. The five factors that affect the separation efficiency of molecular distillation, namely, feed flow rate, distillation temperature, feed temperature, wiper rotating speed, and distillation pressure, are discussed. The optimal recovery condition was determined via orthogonal experiments using an OA(9)(3(4)) design. The IL was recycled and reused 5 times in the homogeneous cellulose acetylation system under optimal conditions. The purity of recycled IL the 5th time reached 99.56%. FT-IR (Fourier transform infrared spectroscopy) and H-1 NMR (nuclear magnetic resonance) spectroscopy showed that the structure of the recovered IL is not changed. This work proves that AmimC1 has excellent reusability, and that molecular distillation is an effective method for recovering IL in homogeneous cellulose acetylation. |
| WOS标题词 | Science & Technology ; Technology |
| 类目[WOS] | Engineering, Chemical |
| 研究领域[WOS] | Engineering |
| 关键词[WOS] | ACETATES ; WATER ; TEMPERATURE ; SEPARATION ; PRODUCTS ; SOLVENT |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000320294300015 |
| 公开日期 | 2015-05-27 |
| 源URL | [http://ir.ipe.ac.cn/handle/122111/13676]  |
| 专题 | 过程工程研究所_研究所（批量导入） |
| 作者单位 | 1.Beijing Univ Technol, Sch Mat Sci & Engn, Beijing 100124, Peoples R China 2.China Acad Sci & Technol Dev, Guangxi Branch, Nanning 530022, Peoples R China 3.Chinese Acad Sci, Inst Proc Engn, Beijing 100190, Peoples R China |
| 推荐引用方式 GB/T 7714 | Huang Kelin,Wu Rui,Cao Yan,et al. Recycling and Reuse of Ionic Liquid in Homogeneous Cellulose Acetylation[J]. CHINESE JOURNAL OF CHEMICAL ENGINEERING,2013,21(5):577-584. |
| APA | Huang Kelin,Wu Rui,Cao Yan,Li Huiquan,&Wang Jinshu.(2013).Recycling and Reuse of Ionic Liquid in Homogeneous Cellulose Acetylation.CHINESE JOURNAL OF CHEMICAL ENGINEERING,21(5),577-584. |
| MLA | Huang Kelin,et al."Recycling and Reuse of Ionic Liquid in Homogeneous Cellulose Acetylation".CHINESE JOURNAL OF CHEMICAL ENGINEERING 21.5(2013):577-584. |
入库方式： OAI收割
来源：过程工程研究所
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