Fast analysis of triterpenoids in Ganoderma lucidum spores by ultra-performance liquid chromatography coupled with triple quadrupole mass spectrometry
文献类型：期刊论文
| 作者 | Yan, Zhou1,2; Xia, Bing2; Qiu, Ming Hua3; Sheng, Ding Li2; Xu, Hong Xi1 |
| 刊名 | BIOMEDICAL CHROMATOGRAPHY
 |
| 出版日期 | 2013-11-01 |
| 卷号 | 27期号:11页码:1560-1567 |
| 关键词 | Ganoderma lucidum spores triterpenoid multiple reaction monitoring daughter ion scan experiment |
| 英文摘要 | A rapid and reliable method was established for simultaneous determination of main triterpenoids in Ganoderma lucidum spores using ultra-high-performance liquid chromatography coupled with triple quadrupole mass spectrometry (UPLC-TQ-MS). The established method was validated in terms of linearity, sensitivity, precision, accuracy and stability, and was successfully applied to determine the contents of 10 main triterpenoids in different batches of G. lucidum spores. The analysis results showed that moderate levels of triterpenoids were found in G. lucidum spores. In addition, a MS full scan with a daughter ion scan experiment was performed to identify the potential derivatives of triterpenoids present in G. lucidum spores. As a result, a total of 22 triterpenoids from different G. lucidum spores were unequivocally or tentatively identified via comparisons with authentic standards and literatures. This method provides both qualitative and quantitative results without the need for repetitive UPLC-MS analyses, thereby increasing efficiency and productivity, making it suitable for high-throughput applications. Copyright (c) 2013 John Wiley & Sons, Ltd. |
| WOS标题词 | Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences |
| 类目[WOS] | Biochemical Research Methods ; Biochemistry & Molecular Biology ; Chemistry, Analytical ; Pharmacology & Pharmacy |
| 研究领域[WOS] | Biochemistry & Molecular Biology ; Chemistry ; Pharmacology & Pharmacy |
| 关键词[WOS] | PROTEASE ; HPLC ; MS |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000328324100026 |
| 源URL | [http://ir.kib.ac.cn/handle/151853/19239]  |
| 专题 | 昆明植物研究所_植物化学与西部植物资源持续利用国家重点实验室 |
| 作者单位 | 1.Shanghai Univ Tradit Chinese Med, Shanghai 201203, Peoples R China 2.Chinese Acad Sci, Chengdu Inst Biol, Chengdu 610041, Peoples R China 3.Chinese Acad Sci, Kunming Inst Bot, Kunming 650201, Peoples R China |
| 推荐引用方式 GB/T 7714 | Yan, Zhou,Xia, Bing,Qiu, Ming Hua,et al. Fast analysis of triterpenoids in Ganoderma lucidum spores by ultra-performance liquid chromatography coupled with triple quadrupole mass spectrometry[J]. BIOMEDICAL CHROMATOGRAPHY,2013,27(11):1560-1567. |
| APA | Yan, Zhou,Xia, Bing,Qiu, Ming Hua,Sheng, Ding Li,&Xu, Hong Xi.(2013).Fast analysis of triterpenoids in Ganoderma lucidum spores by ultra-performance liquid chromatography coupled with triple quadrupole mass spectrometry.BIOMEDICAL CHROMATOGRAPHY,27(11),1560-1567. |
| MLA | Yan, Zhou,et al."Fast analysis of triterpenoids in Ganoderma lucidum spores by ultra-performance liquid chromatography coupled with triple quadrupole mass spectrometry".BIOMEDICAL CHROMATOGRAPHY 27.11(2013):1560-1567. |
入库方式： OAI收割
来源：昆明植物研究所
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