Identification of Three Novel Polyphenolic Compounds, Origanine A-C, with Unique Skeleton from Origanum vulgare L. Using the Hyphenated LC-DAD-SPE-NMR/MS Methods
文献类型：期刊论文
| 作者 | Liu, Hongbing1,4; Zheng, Anmin1; Liu, Huili1; Yu, Haiyan1; Wu, Xiangyu1,4; Xiao, Chaoni1,2; Dai, Hui1,3; Hao, Fuhua1 ; Zhang, Limin1; Wang, Yulan1
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| 刊名 | JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
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| 出版日期 | 2012-01-11 |
| 卷号 | 60期号:1页码:129-135 |
| 关键词 | Origanum vulgare L. polyphenolic compounds cyclohexenetetracarboxylic acids LC-DAD-SPE-NMR/MS origanine A-C computational calculations |
| 英文摘要 | Identification of new compounds especially those with new skeletons from plant kingdom has long been a vital aspect for understanding phytochemistry, plant metabolisms and discovering new bioactive compounds. In this study, we identified and isolated three novel polyphenolic compounds, origanine A-C, from a well-researched plant Origanum vulgare L. using the hyphenated LC-DAD-SPE-NMR/MS methods. Based on the combined information from UV-visible, accurate mass and 2D NMR spectra together with computational calculations, we found that these compounds all had a novel skeleton of cyclohexenetetracarboxylic acids attached with some well-known bioactive moieties including 3,4-dihydroxyphenyl, 4-(beta-D-glucopyranosyloxy)benzyl alcohol (gastrodin), and 3-(3,4-dihydroxyphenyl)lactic acid (danshensu) residues. These findings provided crucial information to fill the gaps in our knowledge in terms of the plant secondary metabolism. This study also indicated the necessity for further research in plant secondary metabolism for even well-studied plants and demonstrated the powerfulness of the hyphenated LC-DAD-SPE-NMR/MS methods for comprehensive analysis of plant metabolites in particular for discovering new natural compounds. |
| WOS标题词 | Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences |
| 类目[WOS] | Agriculture, Multidisciplinary ; Chemistry, Applied ; Food Science & Technology |
| 研究领域[WOS] | Agriculture ; Chemistry ; Food Science & Technology |
| 关键词[WOS] | ACID-DERIVATIVES ; GLUCOSIDE ; OREGANO ; PLANT |
| 收录类别 | SCI ; IC |
| 语种 | 英语 |
| WOS记录号 | WOS:000298943000020 |
| 公开日期 | 2015-07-14 |
| 源URL | [http://ir.wipm.ac.cn/handle/112942/1673]  |
| 专题 | 武汉物理与数学研究所_磁共振应用研究部 |
| 作者单位 | 1.Chinese Acad Sci, Wuhan Inst Phys & Math, Wuhan Ctr Magnet Resonance, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan 430071, Peoples R China 2.NW Univ Xian, Coll Life Sci, Xian 710069, Peoples R China 3.Peking Univ, Dept Physiol & Pathophysiol, Beijing 100191, Peoples R China 4.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China |
| 推荐引用方式 GB/T 7714 | Liu, Hongbing,Zheng, Anmin,Liu, Huili,et al. Identification of Three Novel Polyphenolic Compounds, Origanine A-C, with Unique Skeleton from Origanum vulgare L. Using the Hyphenated LC-DAD-SPE-NMR/MS Methods[J]. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY,2012,60(1):129-135. |
| APA | Liu, Hongbing.,Zheng, Anmin.,Liu, Huili.,Yu, Haiyan.,Wu, Xiangyu.,...&Tang, Huiru.(2012).Identification of Three Novel Polyphenolic Compounds, Origanine A-C, with Unique Skeleton from Origanum vulgare L. Using the Hyphenated LC-DAD-SPE-NMR/MS Methods.JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY,60(1),129-135. |
| MLA | Liu, Hongbing,et al."Identification of Three Novel Polyphenolic Compounds, Origanine A-C, with Unique Skeleton from Origanum vulgare L. Using the Hyphenated LC-DAD-SPE-NMR/MS Methods".JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY 60.1(2012):129-135. |
入库方式： OAI收割
来源：武汉物理与数学研究所
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