Selective saturation and inversion of multiple resonances in high-resolution solid-state C-13 experiments using slow spinning CP/MAS and tailored DANTE pulse sequences
文献类型：期刊论文
| 作者 | Hu, Jian Zhi2; Pugmire, Ronald J.1; Orendt, Anita M.2; Grant, David M.2; Ye, C.3 |
| 刊名 | SOLID STATE NUCLEAR MAGNETIC RESONANCE
 |
| 出版日期 | 1992-11-01 |
| 卷号 | 1期号:4页码:185-195 |
| 关键词 | DANTE CP/MAS chemical shift tensors coal |
| 英文摘要 | Taking advantage of the long C-13 T-1 values generally encountered in solids, selective saturation and inversion of more than one resonance in C-13 CP/MAS experiments can be achieved by sequentially applying several DANTE pulse sequences centered at different transmitter frequency offsets. A new selective saturation pulse sequence is introduced composed of a series of 90 degrees DANTE sequences separated by interrupted decoupling periods during which the selected resonance is destroyed. Applications of this method, including the simplification of the measurement of the principal values of the C-13 chemical shift tensor under slow MAS conditions, are described. The determination of the aromaticity of coal using a relatively slow MAS rate is also described. |
| WOS标题词 | Science & Technology ; Physical Sciences ; Technology |
| 类目[WOS] | Chemistry, Physical ; Physics, Atomic, Molecular & Chemical ; Physics, Condensed Matter ; Spectroscopy |
| 研究领域[WOS] | Chemistry ; Physics ; Spectroscopy |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000208537300003 |
| 公开日期 | 2015-07-28 |
| 源URL | [http://ir.wipm.ac.cn/handle/112942/4656]  |
| 专题 | 武汉物理与数学研究所_2011年以前论文发表（包括2011年） |
| 作者单位 | 1.Univ Utah, Dept Fuels Engn, Salt Lake City, UT 84112 USA 2.Univ Utah, Dept Chem, Salt Lake City, UT 84112 USA 3.Chinese Acad Sci, Wuhan Inst Phys, Wuhan 430071, Peoples R China |
| 推荐引用方式 GB/T 7714 | Hu, Jian Zhi,Pugmire, Ronald J.,Orendt, Anita M.,et al. Selective saturation and inversion of multiple resonances in high-resolution solid-state C-13 experiments using slow spinning CP/MAS and tailored DANTE pulse sequences[J]. SOLID STATE NUCLEAR MAGNETIC RESONANCE,1992,1(4):185-195. |
| APA | Hu, Jian Zhi,Pugmire, Ronald J.,Orendt, Anita M.,Grant, David M.,&Ye, C..(1992).Selective saturation and inversion of multiple resonances in high-resolution solid-state C-13 experiments using slow spinning CP/MAS and tailored DANTE pulse sequences.SOLID STATE NUCLEAR MAGNETIC RESONANCE,1(4),185-195. |
| MLA | Hu, Jian Zhi,et al."Selective saturation and inversion of multiple resonances in high-resolution solid-state C-13 experiments using slow spinning CP/MAS and tailored DANTE pulse sequences".SOLID STATE NUCLEAR MAGNETIC RESONANCE 1.4(1992):185-195. |
入库方式： OAI收割
来源：武汉物理与数学研究所
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。