Determination of Synthetic Musk Fragrances in Sewage Sludge, Sediment and Soil Using Accelerated Solvent Extraction with Gas Chromatography-Mass Spectrometry
文献类型：期刊论文
| 作者 | Hu Zheng-Jun ; Shi Ya-Li ; Cai Ya-Qi |
| 刊名 | CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
 |
| 出版日期 | 2010-06 |
| 卷号 | 38期号:6页码:885-888 |
| 关键词 | Accelerated solvent extraction Synthetic musks Sewage sludge Soil Silica gel/neutral aluminum oxide column Gas chromatography-mass spectrometry |
| 中文摘要 | A rapid, simple accelerated solvent extraction (ASE) method has been developed to determine seven synthetic musks in sewage sludge, sediment and soil by GC-MS. After extraction, samples were cleaned up by silica gel/ neutral Al(2)O(3)column. Then final eluate was concentrated before injection. Identification was carried out by GC-MS in the Selective Ion Monitor (SIM) mode. Using the method, the recovery of fluenthene-d(10), surrogate standard, was from 89.7% to 110.9%. The detection limits of musks were from 2.9 to 3.3 mu g/kg in sewage sludge and 0.25 - 0.33 mu g/kg in sediment and soil (S/N = 3). Using hexachlorobenzene (HCB) (13)C(6) as the internal standard, good linear calibrations were obtained in the range of 0.6 - 100 mu g/kg. The average recoveries were in the range of 83.6% - 105.1% when the spiked concentration was 10 mu g/kg. The RSD ranged from 3.2% to 9.8%. The method is accurate during the inspection of synthetic musks in real samples. |
| WOS记录号 | WOS:000279604300025 |
| 源URL | [http://ir.rcees.ac.cn/handle/311016/21067]  |
| 专题 | 生态环境研究中心_环境化学与生态毒理学国家重点实验室 |
| 推荐引用方式 GB/T 7714 | Hu Zheng-Jun,Shi Ya-Li,Cai Ya-Qi. Determination of Synthetic Musk Fragrances in Sewage Sludge, Sediment and Soil Using Accelerated Solvent Extraction with Gas Chromatography-Mass Spectrometry[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2010,38(6):885-888. |
| APA | Hu Zheng-Jun,Shi Ya-Li,&Cai Ya-Qi.(2010).Determination of Synthetic Musk Fragrances in Sewage Sludge, Sediment and Soil Using Accelerated Solvent Extraction with Gas Chromatography-Mass Spectrometry.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,38(6),885-888. |
| MLA | Hu Zheng-Jun,et al."Determination of Synthetic Musk Fragrances in Sewage Sludge, Sediment and Soil Using Accelerated Solvent Extraction with Gas Chromatography-Mass Spectrometry".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 38.6(2010):885-888. |
入库方式： OAI收割
来源：生态环境研究中心
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。