Trace Analysis of Fifteen Androgens in Environmental Waters by LC-ESI-MS-MS Combined with Solid-Phase Disk Extraction Cleanup
文献类型：期刊论文
| 作者 | Sun, Li; Liu, Yan; Chu, Xiaogan; Lin, Jin-Ming |
| 刊名 | CHROMATOGRAPHIA
 |
| 出版日期 | 2010-05 |
| 卷号 | 71期号:3页码:867-873 |
| 关键词 | Column liquid chromatography ESI-MS-MS Solid-phase disk extraction Environmental water Androgens |
| 中文摘要 | A rapid and sensitive liquid chromatography-electrospray tandem mass spectrometry method, combined with solid-phase disk extraction cleanup, was developed and applied to the analysis of fifteen androgens in waste water. Compounds included androstenedione, androstanolone, boldenone, clostebol, danazol, 6-dehydronandrolone acetate, fluoxymesterone, methyltestosterone, nandrolone, nandrolone propionate, testosterone, testosterone acetate, testosterone propionate, trenbolone and trenbolone acetate, respectively. The overall method recoveries ranged from 78.0 to 107.7% and the limits of detection for the fifteen analytes determined in influent samples were between 0.5 and 4 ng L(-1). The analysis of residual androgens was carried out in waste water obtained from the Beijing area and five analytes (androstenedione, fluoxymesterone, methyltestosterone, testosterone and nandrolone) could be detected in levels ranging from 1.6-3.5, 7.6-66.7, 4.1-7.0, 1.2-4.3 and 1.7 ng L(-1), respectively. |
| WOS记录号 | WOS:000277595400017 |
| 源URL | [http://ir.rcees.ac.cn/handle/311016/21163]  |
| 专题 | 生态环境研究中心_环境化学与生态毒理学国家重点实验室 |
| 推荐引用方式 GB/T 7714 | Sun, Li,Liu, Yan,Chu, Xiaogan,et al. Trace Analysis of Fifteen Androgens in Environmental Waters by LC-ESI-MS-MS Combined with Solid-Phase Disk Extraction Cleanup[J]. CHROMATOGRAPHIA,2010,71(3):867-873. |
| APA | Sun, Li,Liu, Yan,Chu, Xiaogan,&Lin, Jin-Ming.(2010).Trace Analysis of Fifteen Androgens in Environmental Waters by LC-ESI-MS-MS Combined with Solid-Phase Disk Extraction Cleanup.CHROMATOGRAPHIA,71(3),867-873. |
| MLA | Sun, Li,et al."Trace Analysis of Fifteen Androgens in Environmental Waters by LC-ESI-MS-MS Combined with Solid-Phase Disk Extraction Cleanup".CHROMATOGRAPHIA 71.3(2010):867-873. |
入库方式： OAI收割
来源：生态环境研究中心
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